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Original Articles

trans-1-CHLORO-5(ETHOXYETHOXY)-2-PENTENE

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Pages 209-216 | Received 15 Aug 1980, Published online: 12 Feb 2009

References

  • Janssen , C. G. M. , van Lier , P. M. , Schipper , P. , Simons , L. H. J. G. and Godefroi , E. F. 1980 . J. Org. Chem. , 45 : 3195
  • Becher , J. 1972 . Acta Chem. Scand. , 26 : 3627
  • Bohlmann , F. , Weber , D. and Zdero , C. 1973 . Chem. Ber. , 106 : 2745
  • Borch , R. F. , Evans , A. J. and Wade , J. J. 1956 . J. Am. Chem. Soc. , : 126
  • Rossi , R. and Carpita , A. 1977 . Synthesis , : 561
  • Okui , S. , Matsumoto , T. and Takahashi , A. Jap. Patent 4716 . 1961 . Chem. Abstr., 58, Ploo78h (1963)
  • Eaton , P. E. , Cooper , G. F. , Johnson , R. C. and Muller , R. H. 1972 . J. Org. Chem. , 37 : 1947 Dichloroacetic acid-catalyzed addition of 3-bromopropan-l-ol to ethyl vinyl ether has been reported;
  • Chladek , S. and Smrt , J. 1964 . Chem. Ind. (London) , : 1719
  • Collington , E. W. and Meyers , A. I. 1971 . J. Org. Chem. , 36 : 3044
  • See ref. 11; suspected thermal instability of IVa necessitated our having to rely on 1H-NMR inspection rather than on GLC assay for determination of purity
  • Brandsma , L. 1971 . “Preparative Acetylenic Chemistry” , 177 Amsterdam, London, New York : Elsevier Publishing Company .
  • de Haan , J. W. and van de Ven , L. J. M. 1973 . Org. Magn. Res. , 5 : 147 The trans geometry was confirmed by the chemical shifts of C1 and C4; see for instance
  • Compound IVa, especially when crude, appears to be heat sensitive and has, in our hands, decomposed during distillation at bath temperatures exceeding 120°

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