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Original Articles

A MODIFIED PROCEDURE FOR THE PREPARATION OF 5H, 7H-DIBENZO[c,e]SELENEPIN

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Pages 270-274 | Received 10 Jan 1985, Published online: 10 Feb 2009

References

  • Truce , W. E. and Emrick , D. D. 1956 . T. Am. Chem. Soc , 7 : 6130
  • Hall , D. N. , Leslie , N. S. and Turner , E. E. 1950 . J. Chem. Soc , 711
  • Bird , N. L. and Challenger , F. 1939 . J. Chem. Soc , 570
  • 1976 . “The Merck Index”, , 9th Ed. , 633 Rahway, NJ : Merck and Co. Inc. .
  • Calcd for CjjHjjISe: C, 44.91 H, 3.77; I, 31.64. Found: C, 44.67 H, 3.70 I, 30.33
  • Truce , W. E. (personal communication) suggests the more reasonable conceptual structure VII for a product that might arise from incorporation of two equivalents of methyl iodide into the selenepin V; he also presumes the mp of 95–96° recorded here to be correct

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