References
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- Pfeiffer , G. J. and Adkins , H. 1931 . J. Am. Chem. Soc. , 53 : 1043 ]. 2,2-Dimethoxybutane was prepared by a procedure modified from Pfeiffer and Adkin's method because direct application of this method gave a mixture of the ketal and the excess reagent trimethyl orthoformate which were difficult to separate because their close boiling points. In our case, one equivalent trimethyl orthoformate was used to give 2,2-dimethoxybutane in 83% yield
- Young , W. G. , Caserio , F. F. Jr. and Brandon , D. D. Jr. 1960 . J. Am. Chem. Soc. , 82 : 6163
- Booth , H. , King , F. E. and Parrick , J. 1958 . J. Chem. Soc. , : 2302