Lithium Chloride–Assisted Selective Hydrolysis of Methyl Esters Under Microwave Irradiation

REFERENCES

• Biswanath Das , K. V. ; Srinivas , N. S. Conversion of berberine into berberinerrubine by selective demethylation under microwave irradiation . Synth. Commun. 2002 , 32 , 3027 – 3029 .
   Web of Science ®Google Scholar
• Oussaïd , A. ; Thach , L. N. ; Loupy , A. Selective dealkylations of alkyl aryl ethers in heterogeneous basic media under microwave irradiation . Tetrahedron Lett. 1997 , 38 , 2451 – 2454 .
   Web of Science ®Google Scholar
• Bernard , A. M. ; Ghiani , M. R. ; Piras , P. P. ; Rivoldini , A. Dealkylation of activated alkyl aryl ethers using lithium chloride in dimethylformamide . Synthesis 1989 , 4 , 287 – 294 .
   Google Scholar
• Ramesh , P. ; Srividhya , C. Microwave-assisted clay-catalyzed selective demethylation of polymethoxyflavones . Indian J. Hetero. Chem. 2005 , 15 , 157 .
   Web of Science ®Google Scholar
• Xin , J. Y. ; Zhao , Y. J. ; Zhao , G. L. ; Zheng , Y. ; Sheng , X. ; Xia , C. G. ; Li , S. B. Enzymatic resolution of (R, S)-naproxen in water-saturated ionic liquid . Biocatal. Biotransform . 2005 , 23 ( 5 ), 353 – 361 .
   Web of Science ®Google Scholar
• Gill , I. ; Pastor , E. ; Ballesteros , A. Lipase-silicone biocomposites: Efficient and versatile immobilized biocatalysts . J. Am. Chem. Soc. 1999 , 121 ( 41 ), 9487 – 9496 .
   Web of Science ®Google Scholar
• Bond , G. ; Moyes , R. B. ; Theaker , Y. ; Whan , D. A. The effect of microwave heating on the reaction of propan-2-ol over alkalized carbon catalysts . Top. Catal. 1994 , 1 , 177 .
   Web of Science ®Google Scholar
• Villemin , D. ; Labiad , B. ; Loupy , A. Clay catalysis: A convenient and rapid formation of anhydride from carboxylic acid and isopropenyl acetate under microwave irradiation. Synth. Commun. 1993, 23, 419.
   Web of Science ®Google Scholar
• Lidströ , P. ; Tierney , J. ; Wathey , B. ; Westman , J. Microwave assisted organic synthesis . Tetrahedron 2001 , 57 , 9225 – 9283 .
   Web of Science ®Google Scholar
• Larhed , M. ; Hallberg , A. Microwave-assisted high-speed chemistry: A new technique in drug discovery . Drug Discov. Today 2001 , 6 , 406 – 416 .
   PubMed Web of Science ®Google Scholar
• Perreux , L. ; Loupy , A. Effect of cations, substrates and temperature on the microwave-assisted saponification of benzoic and mesitoic esters . Org. Prep. Proced. Int. 2002 , 35 ( 4 ), 361 – 368 .
   Web of Science ®Google Scholar
• Andre , L. ; Philippe , P. ; Mohamed Ramdaniand , P. J. Solid–liquid phase-transfer catalysis without solvent coupled with microwave irradiation: A quick and efficient method for saponification of esters . Synth. Commun. 1994 , 24 ( 2 ), 159 – 165 .
   Web of Science ®Google Scholar
• Brindaban , C. R. ; Pinak , D. ; Arunkanti , S. An efficient and general method for ester hydrolysis on the surface of silica gel catalyzed by indium triiodide under microwave irradiation . Synth.Commun. 2000 , 30 ( 22 ), 4167 – 4171 .
   Web of Science ®Google Scholar
• Kabalka , G. W. ; Wang , L. ; Pagni , R. M. Potassium fluoride doped alumina: An effective reagent for ester hydrolysis under solvent free conditions . Green Chem. 2001 , 3 ( 5 ), 261 – 262 .
   Web of Science ®Google Scholar
• Beil. 9 , 92 .
   Google Scholar
• Beil. 9 , 413 .
   Google Scholar
• Beil. 9 , 389 .
   Google Scholar
• Beil. 10 , 154 .
   Google Scholar
• Beil. 10 ( 1 ), 188 .
   Google Scholar
• Beil. 9 , 573 .
   Google Scholar
• The Merck Index , 10 , 863 .
   Google Scholar
• Beil. 9 , 841 .
   Google Scholar
• Mingos , D. M. P. ; Baghurst , D. R. ; Kingston , H. M. ; Haswell , S. J. (Eds.) Microwave Enhanced Chemistry ; American Chemical Society : Washington , DC , 1997 .
   Google Scholar
• Gedye , R. N. ; Smith , F. E. ; Westaway , K. C. Rate enhancement of organic reactions by microwaves at atmospheric pressure . Can. J. Chem. 1998 , 76 , 525 .
   Web of Science ®Google Scholar
• Carrillo-Munoz , J. R. ; Bouver , D. ; Guibe-Jampel , E. ; Loupy , A. ; Petit , A. Microwave-promoted lipase-catalyzed reactions: Resolution of (±)-1-phenylethanol . J. Org. Chem. 1996 , 61 , 7746 – 7749 .
   PubMed Web of Science ®Google Scholar