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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 39, 2009 - Issue 21
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Original Articles

Synthesis of 3-Methyl-2,6-dimethylbicyclo[3.3.1]nonane-exo-2,exo-6-diol

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Pages 3934-3939 | Received 30 Aug 2008, Published online: 07 Oct 2009

REFERENCES

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  • MacNicol , D. D. ; Toda , F. ; Bishop , R. Comprehensive Supramolecular Chemistry ; Pergamon : Oxford , 1996 ; vol. 4 , p. 85 .
  • Bishop , R. ; Choudhury , S. ; Dance , I. The syntheses and crystal structures of exo-2,exo-6-dihydroxybicyclo[3.3.1]-nonane which do not contain the host helical canals of crystalline exo-2,exo-6-dihydroxy-2,6-dimethyl-bicyclo[3.3.1]nonane . J. Chem. Soc. Perkin Trans. 1 1982 , 9 , 1159 .
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  • Ung , A. T. ; Gizachew , D. ; Bishop , R. Structure and analysis of helical tubulate inclusion compounds formed by 2,6-dimethylbicyclo[3.3.1]nonane-exo-2,exo-6-diol . J. Am. Chem Soc. 1995 , 117 , 8745 .
  • Quast , H. ; Görlach , Y. ; Stawitz , J. Verbesserte Herstellung des Meerwein-Esters und Struktur neutraler Nebenprodukte: 1,1,3,3,5-Cyclohexan-pentacarbon-säure-pentamethylester and 1-Piperidincarbonsäure methylester. Liebigs Ann. Chem. 1985, 1653–1658.
  • Quast , H. ; Witzel , M. Synthesis of tetramethyl 2,6-dihydroxybicyclo[3.3.1]nona-2,6-diene-1,3,5,7-tetracarboxylate (Meerwein Ester)—Use of tert-butyl methyl ether instead of benzene in azeotropic distillation . Liebigs Ann. Chem. 1993 , 699 .
  • Schaefer , J. P. ; Hoing , L. M. Bicyclo[3.3.1]nonanes, IV: Dehydration of the bicyclo[3.3.1]nonane-2,6-diols . J. Org. Chem. 1968 , 33 , 2655 .
  • Meerwein , H. ; Kiel , F. ; Klosgen , G. The synthesis of Meerwein's ester . J. Prakt. Chem. 1922 , 104 , 161 .

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