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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 2, 1972 - Issue 3
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Original Articles

A Stereospecific Swihesis of 6-sanialene

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Pages 165-169 | Received 03 Mar 1972, Published online: 26 Jan 2007

References

  • 1966–1969 . National Science Foundation Predoctoral Fellow
  • 1969–1971 . Purdue David Ross Fellow
  • Corey , E. J. , Hartasn , R. and Vatakmcheny , P. A. J. Amer. Chem. Sec. , 84 2611 See, for a synthesis of 8-santalene; and H. C. Kretscbaar and W. P. Eraan, Tetrahedron Letters., 41 (1970) for the synthesis of B-santalol
  • Kolinsky , J. , Dinmel , D. R. and Gibson , T. W. 1967 . J. Org. Chem. , 32 : 2087
  • When the reaction of camphene sultone with n-butyllithim was conducted at a higher temperature attack at sulfur leading to a hydroxy butylsulfone predominated
  • Molecular models show that the methyl group in 5 approaches the carbon-carbon double bond; consequently, we tentatively assign structure 5 to the isomer melting at 62 since it displays an upfield methyl signal

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