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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 3, 1973 - Issue 2
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Original Articles

The Synthesis of Some 9-,10-, and 11-Membered Ring Compounds Containing a Nitrogen Atom: 2,3,4,5,6,7-Hexahydro-1H-3-Benzazonines, 1,2,3,4,5,6,7,8-Octahydro-3-Benzazocines, and 2,3,4,5,6,7,8,9-Octahydro-1H-3-Benzazacy-cloundecanes

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Pages 153-160 | Received 20 Feb 1973, Published online: 06 Dec 2006

References

  • Pecherer , B. , Sunbury , R. C. and Brossi , A. 1972 . J. Heterocyclic Chem. , 9 : 609
  • Pecherer , B. , Stumpf , J. and Brossi , A. 1970 . Helv. Chem. Acta , 53 : 763
  • Pecherer , B. , Humiec , F. and Brossi , A. 1971 . Helv. Chem. Acta , 54 : 743
  • Pecherer , B. , Sunbury , R. C. , Humiec , F. and Brossi , A. 1971 . XXIII IUPAC Congress . July 26–30 1971 , Boston, Mass.. pp. 63 Paper No. 155
  • Pecherer , B. , Humiec , F. and Brossi , A. 1972 . Synth, Comm. , 2 : 315
  • Cope , A. C. and LeBel , N. 1960 . J. Amer. Chem. Soc. , 82 : 4656
  • All melting points were taken in open capillaries with a Thomas-Hoover melting point apparatus and are uncorrected. Nmr spectra were obtained with a Varian A-60 spectrometer using tetramethylsilane as the internal standard. Mass spectra were obtained on a CEC 21–110 spectrometer with direct introduction of the sample, at 70eV. The yields of all compounds are those of isolated products, homogeneous on tlc; all compounds gave acceptable elemental analyses
  • English , J. , Barber , G. W. and Lapides , L. J. 1948 . J. Amer. Chem. Soc. , 70 : 2860
  • Cason , J. 1955 . Org. Syntheses Coll. , Vol. III , 169 N. Y., N. Y. : John Wiley & Sons .
  • Depending upon the state of the resin, this volume may vary. On occasion 8 column volumes have been required for complete recovery

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