Publication Cover
Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 6, 1976 - Issue 8
11
Views
11
CrossRef citations to date
0
Altmetric
Original Articles

A Convenient Synthesis and Resolution of R- and S- Atrolactic Acid in High Enantiomeric Purity

&
Pages 601-608 | Received 24 Sep 1976, Published online: 05 Dec 2006

References

  • Prelog , V. 1953 . Helv. Chim. Acta , 36 : 308 Bull. Soc. Chim. (France), 987 (1956)
  • Morrison , J. D. and Mosher , H. S. 1971 . “ Ch. 2 ” . In Asymmetric Organic Reactions , Englewood Cliffs, N. J. : Prentice-Hall .
  • Meyers , A. I. and Mihelich , E. D. 1976 . Angew. Chem. Int. Ed. , 15 : 270
  • Meyers , A. I. , Knaus , G. , Kamata , K. and Ford , M. E. 1976 . J. Am. Chem. Soc. , 98 : 567
  • Meyers , S. I. , Davis , L. , Temple , Robert , Nolen , L. and Edward , D. Mihelich . 1974 . J. Org. Chem. , 39 : 2778
  • Preparative liquid chromatography using medium pressure was carried out at 90 psi using a 25 × 1000 mm Altex column containing ICN silica gel, .032-.060 mm, Woelm type 206. The sample capacity of this column is 10–12 grams and the purified material was collected after elution with 30% acetone-hexane
  • McKenzie , A. and Clough , G. W. 1910 . J. Chem. Soc. , 97 : 1019 Based on [α]13 D +37.3° report [α]20 D +35. 3° via resolution. R. Barnes and B. Juliana, J. Am. Chem. Soc., 81, 6462 (1959)

Reprints and Corporate Permissions

Please note: Selecting permissions does not provide access to the full text of the article, please see our help page How do I view content?

To request a reprint or corporate permissions for this article, please click on the relevant link below:

Academic Permissions

Please note: Selecting permissions does not provide access to the full text of the article, please see our help page How do I view content?

Obtain permissions instantly via Rightslink by clicking on the button below:

If you are unable to obtain permissions via Rightslink, please complete and submit this Permissions form. For more information, please visit our Permissions help page.