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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 6, 1976 - Issue 3
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Original Articles

A Convenient Synthesis OF 2-Carbomethoxycyclohexanone

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Pages 169-174 | Received 25 Nov 1975, Published online: 13 Dec 2006

References

  • To whom correspondence should be addressed
  • Fichter , F. and Simon , C. 1934 . Helv. Chim. Acta , 17 : 1218
  • Levine , R. and Hauser , C. R. 1944 . J. Amer. Chem. Soc. , 66 : 1768
  • Bachmann , W. E. , Fujimoto , G. I. and wick , L. B. 1950 . J. Amer. Chem. Soc. , 72 : 1995
  • 2-Carbomethoxycyclohexanone is commercially available as a mixture (1:1) with 2-carbethoxycyclohexanone.
  • Bouveault , L. and Locquin , R. 1908 . Compte Rend. , 146 : 138
  • Walther , H. , Treibs , W. and Michaelis , K. 1956 . Chem. Ber. , 89 : 60
  • Banus , M. D. and Hinckley , A. A. 1957 . Handling and uses of the Alkali Metals . Amer. Chem. Soc. , : 106 Advan. Chem. Ser., No 19
  • Krapcho , A. P. , Diamanti , J. , Cayen , C. and Bingham , R. 1967 . Org. Synt. , 41 : 22
  • Snyder , H. R. , Brooks , L. A. and Shapiro , S. H. 1943 . Org. Synt. Coll. , Vol. II : 531
  • Shahak , I. 1966 . Tetrahedron Lett. , : 2201
  • Munk , P. and Plesek , J. 1957 . Chem. Listy , 51 : 633 Chem. Abst. 51, 11261c (1957); also Org. Reactions, Vol. 16, 67 (1968).
  • Pithia , J. , Tilichenko , M. N. and Kharchenko , V. G. 1964 . Zh. Obshch. Khim. , 34 : 1936 Chem. Abst. 61, 8163g (1964); also Org. Reactions, Vol. 16, 67 (1968).
  • Sodium hydride (99%) available from Alfa Inorganics.
  • Potassium hydride (35% in oil) was supplied by Alfa Products, Beverly, Massachusetts and was washed five times with dry hexane before use.

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