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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 6, 1976 - Issue 3
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Original Articles

A New Synthesis and the 13C-NMR OF β-Cyperone 1,3-Dibromo-2-Pentene, A New Ethyl Vinyl Ketone Equivalent

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Pages 209-215 | Received 12 Dec 1975, Published online: 13 Dec 2006

References

  • Gammill , R. B. and Bryson , T. A. 1975 . Tetrahedron Letters , : 3793
  • Compound 4 is readily available from the Farchan Division of the Story Chemical Corporation.
  • Boiling points reported are oven temperatures observed for bulb to bulb distillation.
  • Corey , E. J. , Katzenellenbogen , J. A. and Posner , G. H. 1967 . J. Amer. Chem. Soc. , 89 : 4245
  • Newman , M. S. and Wotig , J. H. 1949 . J. Amer. Chem. Soc. , 71 : 1292
  • Lansbury , P. T. 1972 . Acc. of Chem. Research , Vol : 311
  • Kobayashi , M. and Matsumoto , T. 1973 . Chem. Letters , : 957
  • Pregosin , P. S. , Randall , E. W. and McMurray , T. B. H. 1972 . J. Chem. Soc., Perkin I , : 299 G. P. Moss, P. S. Pregosin and E. W. RAndall, J. Chem. Moc., Perkin I, 1525 (1974).
  • Stothers , J. B. and Lauterbus , P. C. 1964 . Can. J. Chem. , 42 : 1563
  • Marr , D. H. and Stothers , J. B. 1965 . Can. J. Chem. , 43 : 519
  • Grant , D. M. and Paul , E. G. 1964 . J. Amer. Chem. Soc. , 86 : 2984
  • Both bicyclic compounds shown below have been prepared and their 13C-NMR assigned in our laboratory
  • Stothers , J. B. 1972 . “ Carbon-13 NMR Spectroscopy ” . New York : Academic Press .
  • Spectra recorded on a Varian CFT-20 NMR Spectrometer in CDCl3 with TMS as in internal standard.

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