A Convenient in Situ Preparation of Trimethylsilyl Iodide

References

• Jung , M. E. and Lyster , M. A. 1977 . J. Org. Chem. , 42 : 3761 J. Minamikawa and A. Brossi, Tetrahedron Lett., 3085(1978); B. I. Rosen and W. P. Weber, J. Org. Chem., 42, 3463(1977); M. G. Voronkov, E. I. Dubinskaya, V. G. Komarov and S. F. Pavlov, Zh. Obshch. Khim., 46, 1908(1976); M. G. Voronkov, V. E. Puzanova, S. F. Pavlov and E. I. Dubinskaya, Izv. Akad. Nauk SSSR, Ser. Khim., 448(1975)
   Web of Science ®Google Scholar
• Jung , M. E. and Lyster , M. A. 1977 . J. Am. Chem. Soc. , 99 : 968 T.-L. Ho and G. A. Olah, Angew. Chem., 88, 847(1976)
   Web of Science ®Google Scholar
• Blackburn , G. M. and Ingleson , D. 1978 . J. Chem. Soc., Chem. Commun. , : 870
   Google Scholar
• Jung , M. E. and Lyster , M. A. 1978 . J. Chem. Soc., Chem. Commun. , : 315
   Google Scholar
• Jung , M. E. , Andrus , W. A. and Ornstein , P. L. 1977 . Tetrahedron Lett. , : 4175
   Google Scholar
• Olah , G. A. , Gupta , B. G. B. and Narang , S. C. 1977 . Synthesis , : 583 K. C. Nicolaou, W. E. Barnette and R. L. Magolda, J. Am. Chem. Soc., 100, 2567(1978)
   Web of Science ®Google Scholar
• Jung , M. E. , Mazurek , M. A. and Lim , R. M. 1978 . Synthesis , : 588
   Google Scholar
• Jung , M. E. and Ornstein , P. L. 1977 . Tetrahedron Lett. , : 2659
   Google Scholar
• Ho , T.-L. 1979 . Synthetic Commun. , 9 : 233
   Web of Science ®Google Scholar
• Jung , M. E. , Mossman , A. B. and Lyster , M. A. 1978 . J. Org. Chem. , 43 : 3698
   Web of Science ®Google Scholar
• For the preparation of 1 from trimethylsilyl chloride, see M. E. Jung, reference 1. Trimethylsilyl iodide is also commercially available from several suppliers
   Google Scholar
• Ho , T.-L. and Olah , G. A. 1977 . Synthesis , : 417 T.-L. Ho and G. A. Olah, Proc. Natl. Acad. Sci. USA, 75, 4(1978)
   Google Scholar
• Pray , B. O. , Sommer , L. H. , Goldberg , G. M. , Kerr , G. T. , DiGiorgio , P. A. and Whitmore , F. C. 1948 . J. Am. Chem. Soc. , 70 : 433
   Google Scholar
• Jung , M. E. and Blumenkopf , T. A. 1978 . Tetrahedron Lett. , : 3657
   Google Scholar
• Weyenberg , D. R. and Toporcer , L. H. 1960 . J. Am. Chem. Soc. , 84 : 2843
   Web of Science ®Google Scholar
• Morita , T. , Okamoto , Y. and Sakurai , H. 1978 . Tetrahedron Lett. , : 2523 T. Morita, Y. Okamoto and H. Sakurai, J. Chem. Soc., Chem. Commun., 874(1978); Y. Machida, S. Nomoto and I. Saito, Synthetic Commun., 9, 97(1979); A. H. Schmidt and M. Russ, Chem.-Ztg., 102, 26, 65(1978); G. A. Olah, S. C. Narang, B. G. B. Gupta and R. Malhotra, Synthesis, 61(1979); G. A. Olah, S. C. Narang, B. G. B. Gupta and R. Malhotra, J. Org. Chem., 44, 1247(1979)
   Google Scholar
• Seitz , D. E. and Ferreira , L. 1979 . Synthetic Commun. , 9 : 451
   Web of Science ®Google Scholar
• Band , S. J. and Davidson , I. M. T. 1970 . Trans. Farad. Soc. , 66 : 406
   Google Scholar
• 1955 . Chem. Abstr. , 49 : 11542 For a brief description of the solution reaction of 5 and iodine, see
   Google Scholar
• LePage , J. N. , Lindner , W. , Davies , G. , Seitz , D. E. and Karger , B. L. 1979 . Anal. Chem. , 51 : 433 J. N. Le-Page, W. Lindner, G. Davies, D. E. Seitz and B. L. Karger, J. Chromatogr., submitted
   Web of Science ®Google Scholar
• 1975 . “Atlas of Spectral Data and Physical Constants for Organic Compounds” , vol. 3 , 700 CRC Press .
   Google Scholar