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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 10, 1980 - Issue 2
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Original Articles

Phenyldiazenes from Phenyl Diazonium Fluoborate and Carbanions

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Pages 155-160 | Published online: 05 Dec 2006

References

  • Houben-Weil . 1957 . Methoden der Organische Chemie Vol. 11–1 , 805 – 8 .
  • Tamura , Y. , Minambawa , J. and Ikeda , M. 1977 . Synthesis , : 1
  • 1971 . Ref la , 10–1 : 1126 – 27 .
  • Smith , P. A. S. , Rowe , C. D. and Bruner , L. B. 1969 . J. Org. Chem. , 34 : 3430
  • Reactions of enolates and nitroso compounds will be reported shortly. Garst, M. E., and Buss, J., manuscript in preparation
  • Paramerter , S. M. 1959 . Organic Reactions , 10 : 1 – 142 . and Phillips, R. R., Organic Reactions, 143–178
  • Jackson , A. , Wilson , N. D. V. , Gaskell , A. J. and Joule , J. A. 1969 . J. Chem. Soc. (C) , : 2738 and references therein
  • Curtin , D. Y. and Ursprung , J. A. 1956 . J. Org. Chem. , 21 : 1221
  • Normura , Y. 1961 . Bull. Chem. Soc. Japan , 34 : 1648 1962, 35, 111; and 1964, 37, 967 and 970
  • Characterized by the usual spectral methods
  • Gillis , B. T. and Hagarty , J. D. 1965 . J. Am. Chem. Soc. , 87 : 4576 Prepared according to
  • Flood , D. T. 1943 . Org. Synthesis, II , : 295
  • 522 – 545 . For a complete discussion of the numerous reducing agents available see ref la
  • Removal of the aniline is in theory possible in this instance by chromatography or extraction. Thus far we have been unable to prepare 4-diazobenzenesulfonate sufficiently dry for Grignard reactions. Removal of the “aniline” could then be a simple extraction

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