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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 10, 1980 - Issue 2
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Original Articles

Synthesis of 5-Hydroxy-1, 3-Benzoxathiole

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Pages 161-166 | Received 11 Sep 1979, Published online: 05 Dec 2006

References

  • Degani , I. , Dolci , M. , Fochi , R. , Arzone , A. and Vidano , C. Ital. Patent . 23039 . A/79, Italian National Research Council
  • Baum , J. W. U.S. Patent . 3 891 714 . 1973 . Zoecon Corp.; C.A. 83, 113957 (1975)
  • Lau , P. T. S. and Kestner , M. 1968 . J. Org. Chem. , 33 : 4426 H. Burton, S.B. David, J. Chem. Soc. 1952, 2193
  • Huet , F. , Lechevallier , A. , Pellet , M. and Conia , J. M. 1978 . Synthesis , : 63
  • In absence of the stabilizer, the colour of the reaction solution changes from colorless to dark yellow
  • Use of sodium hydrogen carbonate is necessary to avoid a partial hydrolysis of acetal 3, catalyzed by silica gel4,7
  • Brown , J. J. , Lenhard , R. N. and Bernstein , S. 1964 . J. Am. Chem. Soc. , 86 : 2183

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