The Synthesis of Hydroxytrifluoromethyl 3H-Benzazepines

References

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• See ref. 2b for exception
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• Parr Model 4712 with gage block and 45 ml cup
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• The amount of substrate used appears to be limited only by the size of the pressure vessel
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• Under these conditions 300–351 psi was generated
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• Minimum reaction times were not thoroughly investigated
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