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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 10, 1980 - Issue 1
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Original Articles

Monoacetals of α-Dicarbonyl Compounds from Enol Ethers

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Pages 83-87 | Received 16 Aug 1979, Published online: 03 Jan 2007

References

  • Woodward , R. B. , Pachter , I. J. and Schleinbaum , M. L. 1974 . Organic Syntheses , 54 : 37 ibid., 54, 39 (1974); E. J. Corey and S. Knapp, Tetrahedron Letters, 4687 (1976); B. M. Trost and G. S. Massiot, J. Am. Chem. Soc., 99, 4405 (1977); B. M. Trost, Chem. Rev., 78, 363 (1978); Y. Nagao, M. Ochiai, K. Kaneko, A. Maeda, K. Watanabe and E. Fujita, Tetrahedron Letters, 1345 (1977); Y. Nagao, K. Kaneko and E. Fujita, ibid., 4115 (1978); Y. Nagao, K. Kaneko, K. Kawabata and E. Fujita, ibid., 5021 (1978)
  • Cuvigny , T. and Normant , H. 1977 . Synthesis , : 198
  • Huet , F. , Pellet , M. and Conia , J. M. 1976 . Tetrahedron Letters , : 3579 F. Huet, M. Pellet and J. M. Conia, Synthesis, 33 (1979)
  • Cuvigny , T. , Larcheveque , M. and Normant , H. 1978 . Synthesis , : 857
  • Huet , F. , Pellet , M. and Conia , J. M. 1977 . Tetrahedron Letters , : 3505
  • Huet , F. , Lechevallier , A. and Conia , J. M. 1977 . Tetrahedron Letters , : 2521
  • Rousseau , G. , Lechevallier , A. , Huet , F. and Conia , J. M. 1978 . ibid. , : 3287
  • Huet , F. , Lechevallier , A. , Pellet , M. and Conia , J. M. 1978 . Synthesis , : 63
  • Frimer described in ref , A. A. 9∗ preparations of adipoin dimethyl acetal and 2-methoxy-3-hydroxytetrahydropyran by epoxidation in methanol of the corresponding enol ethers
  • Frimer , A. A. 1977 . Synthesis , : 578
  • Ratcliffe , R. and Rodehorst , R. 1970 . J. Org. Chem. , 35 : 4000
  • Epoxidation of mixtures in MeOH gives
  • Wohl , R. A. 1974 . Synthesis , : 38
  • Prepared according to the procedure given in ref,12 with 73%yield, b.p./torr 75°/56
  • Huet , J. 1975 . Thesis, Université de Paris Sud, Orsay
  • Rousseau , G. , Le Perchec , P. and Conia , J. M. 1978 . Synthesis , : 67
  • Henery-Logan , K. R. and Fridinger , T. L. 1968 . J. C. S. Chem. Comm. , : 130 This compound can also be prepared from α,α-dichloroacetophenone according to
  • When starting from crude acyloin acetals the oxidation product, in some cases, is better purified by column chromatography on silicagel

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