Publication Cover
Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 12, 1982 - Issue 6
19
Views
5
CrossRef citations to date
0
Altmetric
Original Articles

The Synthesis and 13C-NMR Spectrum of 1,4-Dioxaspiro(4.5)deca-6,9-dien-2,8-dione

&
Pages 427-430 | Published online: 05 Dec 2006

References

  • Evans , D. A. , Cain , P. A. and Wong , R. Y. 1977 . J. Amer. Chem. Soc. , 99 : 7083 references quoted therein
  • Heller , J. E. , Dreiding , A. S. , O'Connor , B. R. , Simmons , H. E. , Buchanon , G. L. , Raphael , R. A. and Taylor , R. 1973 . Helv. Chim. Acta , 56 : 272
  • Bélanger , A. , Berney , D. J. F. , Borschberg , H.-J. , Brousseau , R. , Doutheau , A. , Durand , R. , Katayama , H. , Lapalme , R. , Leture , D. M. , Liao , C.-C. , Mac , F. N. , Lachlan , J. , Maffrand , P. , Marazza , F. , Martino , R. , Moreau , C. , Saint-Laurent , L. , Saintonge , R. , Soucy , P. , Ruest , L. and Deslongchamps , P. 1979 . Can. J. Chem. , 57 : 3348
  • Atwal , K. S. , Marini-Bettolo , R. , Sanchez , I. H. , Tsai , T. Y. R. and Wiesner , K. 1978 . Can. J. Chem. , 56 : 1102
  • Sobotka , H. and Austin , J. 1952 . J. Amer. Chem. Soc. , 74 : 3813
  • mp (benzene-pentane): softens 58–62, melts 62–64°C. Satisfactory elemental analysis by Guelph Chemical Laboratories Ltd. Infrared: CH2C12; 1820. (lactone), 1685, 1650cm-1 (cyclohexadienone).max Ultraviolet spectrum: ; 220. (logε 3.98) and 244. nm (logε 3.91). 1H-nmr ; 6.33. (2H, d, J=10. Hz) for HA, 6.85. (2H, d, J=10Hz) for HB and 4.55. ppm (2H, s) for HC
  • The financial assistance of the Natural Sciences and Engineering Research Council of Canada and the Research Board of the University of Manitoba is gratefully acknowledged

Reprints and Corporate Permissions

Please note: Selecting permissions does not provide access to the full text of the article, please see our help page How do I view content?

To request a reprint or corporate permissions for this article, please click on the relevant link below:

Academic Permissions

Please note: Selecting permissions does not provide access to the full text of the article, please see our help page How do I view content?

Obtain permissions instantly via Rightslink by clicking on the button below:

If you are unable to obtain permissions via Rightslink, please complete and submit this Permissions form. For more information, please visit our Permissions help page.