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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 13, 1983 - Issue 6
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Original Articles

Improved Preparation of (E)-3-Trimethylsilyl-2-Buten-1-OL

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Pages 531-535 | Published online: 03 Jan 2007

References

  • Stork , G. , Jung , M. E. , Colvin , E. and Noel , Y. 1974 . J. Am. Chem. Soc. , 96 : 3684 – 6 .
  • Corey , E. J. , Katzenellenbogen , J. A. and Posner , G. H. 1967 . J. Am. Chem. Soc. , 89 : 4245 – 7 .
  • Denmark , S. E. and Jones , T. K. 1982 . J. Org. Chem. , 47 : 4595 – 7 . For some recent findings on the reduction methodology in the Stork sequence see
  • Piers , H. , Chung , J. M. and Morton , H. E. 1981 . Tetrahedron Lett. , 22 : 4905 – 8 .
  • Corey , E. J. and Katzenellenbogen , J. A. 1969 . J. Am. Chem. Soc. , 91 : 1851 – 2 . For early work on the addition of organocopper reagents to acetylenic esters see, Siddall, J. B., Biskup, M., Fried, J. H., J. Am. Chem. Soc. 1969, 91, 1853–4
  • Trost , B. M. and Chan , B. M. T. 1982 . J. Am. Chem. Soc. , 104 : 3733 – 5 .
  • Smith , J. G. 1983 . Synthetic Commun. , 13 : 1 – 6 .
  • Fleming , I. and Roessler , F. J. C. S. Chem. Commun. , 1980 276 – 7 .
  • Still , W. C. 1976 . J. Org. Chem. , 41 : 3063 – 4 . Trimethylsilyllithium was prepared according to
  • The 1H NMR spectrum was recorded on a Varian EM-390 instrument employing Me4Si as the internal standard

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