References
- Gupton , J. , Idoux , J. , Colon , C. and Rampi , R. 1982 . Synth. Commun. , 12 : 695
- Idoux , J. , Gupton , J. , McCurry , C. , Crews , A. , Jurss , C. , Colon , C. and Rampi , R. 1983 . J. Org. Chem. , 48 : 3771
- Tiecco , M. , Cogolli , P. , Maiolo , F. , Testaferri , L. and Tingoli , M. 1979 . J. Org. Chem. , 44 : 2642
- Tiecco , M. , Testaferri , L. and Tingoli , M. 1980 . J. Org. Chem. , 45 : 4376
- Bobbitt , J. and Scola , D. 1960 . J. Org. Chem. , 25 : 560 For an example of a similar type of catalytic hydrogenolysis see
- Gerstenberger , M. and Haas , A. 1981 . Angew. Chem. Int. Ed. Engl. , 20 : 647
- Infrared spectra were recorded on either a Perkin Elmer Model 1420 infrared spectrometer or a Nicolet MXS FT IR as thin films or nujol mulls. NMR spectra were obtained in CC14, DCC13, or Me2SO - d6 solutions [(CH3)4 SI internal standard] at 60 MHz with a Varian EM-360 spectrometer. All boiling points and melting points are uncorrected and melting points were recorded on a Fisher-Johns melting-point apparatus
- When polyfluoroalkoxylation was desired, 2.2–3.0 equivalents of sodium hydride and 2,2,2-trifluoroethanol were used relative to the amount of the dihalobenzene substrate