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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 15, 1985 - Issue 7
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Original Articles

The Reaction of Silyl Enol Ethers With Ethyl Azodicarboxylate and 4-Phenyl-1,2,4-Triazoline-3,5-Dione

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Pages 649-655 | Published online: 05 Dec 2006

References

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  • Woodward , R. B. , Hensler , K. , Gosteli , J. , Naegli , P. , Op-polzer , W. , Ramage , R. , Ranganathan , S. and Vorbruggen , H. 1966 . J. Am Chem. Soc. , 88 : 852 In this paper the lead tetracetate oxidation of a hydrazodiester is described
  • We have briefly explored the conversion of 7 and 9 to the α-diazocyclopentanone. A solution of compound 7 (0.01 mole) in methanol (50ml) containing sodium hvpochlorite (5 ml) was stirred at room temperature for 48 hours. After the workup, the ir of the crude reaction mixture shows absorption in the region of 2100 cm−1
  • Hoye , T. R. , Bottorff , K. J. , Caruso , A. J. and Dellaria , J. F. 1980 . J. Org. Chem. , 45 : 4287
  • Shiloff , J. D. and Hunter , N. R. 1976 . Tetrahedron Lett. , : 3723
  • Williams , A. G. and Butler , G. B. 1980 . J. Orq. Chem. , 45 : 1232
  • Hassner , A. , Reuss , R. H. and Pinnick , H. W. 1975 . J. Org. Chem. , 40 : 3427
  • Stickler , J. C. and Pirkle , W. H. 1966 . J. Org. Chem. , 11 : 3444

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