A Convenient Preparation of Certain N, Ndialkylcarbamoyl Chlorides

References

• Takemura , T. 1982 . General Review of Research on Herbicides , Tokyo : Hakuyusha . [Chem. Abstr., 98, B84865 (1983)]
   Google Scholar
• Daescu , C. , Bacaloglu , R. and Ostrongrovicih , G. 1972 . Bul. Stiint. Teh. Politeh. Timisoara, Ser. Chim. , 17 : 103 Cf., [Chem. Abstr., 80, 47426k (1974)]
   Google Scholar
• Böhme , H. , Koch , L. and Köhler , E. 1962 . Chem. Ber. , 95 : 1849
   Google Scholar
• Brircofer , L. and Krebs , K. 1968 . Tetrahedron Lett. , : 885
   Google Scholar
• Hasserodt , U. 1968 . Chem. Ber. , 101 : 113
   Google Scholar
• Saegusa , T. , Tsuda , T. and Isegawa , Y. 1971 . J. Org. Chem. , 36 : 858
   Google Scholar
• Schnidler , N. and Plöger , W. 1971 . Chem. Ber. , 104 : 969
   Google Scholar
• Saito , J. , Tamura , T. and Morishima , N. Japan Kokai . 75 89, 344 . [Chem. Abstr., 83, 205987n (1975)]
   Google Scholar
• Knabe , J. 1954 . Arch. Pharm. , 289 : 479
   Google Scholar
• Cotter , R. J. and Beach , W. F. 1964 . J. Org. Chem. , 29 : 751
   Google Scholar
• von Braun , J. 1903 . Ber. , 36 : 2286
   Google Scholar
• Bp 88°C(23 Torr). IRv(CHCl3):1670cm−1. 1H-NMRδ (CDCl3) (100MHz): 1.19 (12H, d, J=6.9Hz), 1.26 (3H, t, J=7.1Hz), 3.66–4.12 (2H, m), 4.11 (2H, q, J=7.1 Hz). MSm/z:173(M+)
   Google Scholar
• Danne , R. L. 1955 . J. Org. Chem. , 20 : 92
   Google Scholar
• Joullie , M. M. and Day , A. R. 1954 . J. Am. Chem. Soc. , 76 : 2990
   Google Scholar
• Similar reaction (reflux; 2 h) of methyl pyrrolidine-1-carboxylate20) gave 2f in 58% yield
   Google Scholar
• In similar reaction (reflux; 20 h) of methyl morpholine-1-carboxylate21), 2h was not obtained and unchanged starting material was recovered in 75% yield
   Google Scholar
• von Braun , J. 1903 . Ber. , 36 : 2259
   Google Scholar
• Christenson , I. 1964 . Acta Chem. Scand. , 18 : 904
   Google Scholar
• De Oliveria Baptista , M. J. V. , Barrett , A. G. M. , Barton , D. H. R. , Kelly , J. , Papadimitrion , V. J. , Turner , J. V. and Usher , N. A. 1977 . J. Chem. Soc. Perkin I , : 1477
   PubMedGoogle Scholar
• Kita , Y. , Haruta , J. , Tagawa , H. and Tamura , Y. 1980 . J. Org. Chem. , 45 : 4519
   Web of Science ®Google Scholar
• Böhme , H. and Häfner , L. 1966 . Chem. Ber. , 99 : 281
   Google Scholar