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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 17, 1987 - Issue 14
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Original Articles

Triene Cyclizations. The Total Synthesis of Pallescensin A

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Pages 1655-1665 | Published online: 06 Dec 2006

References

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  • Liotta , D. , Saindane , M. and Ott , W. 1983 . Tetrahedron Lett. , : 2473 Ketone 2 was prepared by the reaction of a cis- and trans-mixture of 2,6-dimethylcyclohexanones with lithium diisopropylamide in THF, followed by methyl iodide. Furan 3 was prepared in a two step process (80% overall yield). See
  • Woodward , R. B. and Hoffmann , R. 1965 . J. Amer. Chem. Soc. , 87 : 395
  • This process was initially done by performing the pyrolysis in the presence of trace amounts of acetic acid. However, this method proved inconsistent. We thank Professor Andrew Kende (University of Rochester) for suggesting the use of silica gel in place of acetic acid
  • Liotta , D. , Saindane , M. and Jamison , W. C. L. J. Org. Chem. , submitted

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