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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 18, 1988 - Issue 9
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Original Articles

The Reaction of α-Methylstyrene Analogs and Related Compounds With Sodium Perborate in Acetic Acid

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Pages 937-947 | Published online: 05 Dec 2006

References

  • McKillop , A. and Tarbin , J. 1987 . Tetrahedron , 43 : 1753
  • McKillop , A. and Tarbin , J. 1983 . Tetrahedron Lett. , 24 : 1505
  • Gupton , J. and Layman , W. 1987 . J. Org. Chem. , 52 : 3683
  • A manuscript describing this work is currently being prepared.
  • The trans-l,2-diacectoxycylcohexane was obtained by treating, a sample of trans-cyclohexane-l,2-diol5 with excess acetic anhydride in pyridine at room temperature.
  • We would like to thank Professor Slayton Evans of the University of North Carolina at Chapel Hill for supplying us with a generous sample of this material
  • Infrared spectra were recorded on a Perkin-Elmer Model 1420 infrared spectrometer as either thin films or Nujol mulls. NMR spectra were obtained in CCl4, DCC13, or Me2SO-d6 solutions [(CH33)4SI internal standard] at 60 MHz with a Varian EM-360 spectrometer. Some of the mass spectra were obtained on a Hitachi Perkin-Elmer RMU-6E spectrometer. All boiling points and melting points are uncorrected, and melting points were recorded on a Fisher-Johns melting point apparatus. The organolithium reagents used for this work were purchased from Aldrich Chemical.

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