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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 18, 1988 - Issue 11
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Original Articles

A Comvewiemt Synthesis of 1-Aminopolycycloalkames and Their Tosylate Salts

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Pages 1179-1186 | Published online: 06 Dec 2006

References

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  • Feldmann , G. and Kirmse , W. 1987 . Angew. Chem. Int. Ed. Engl. , 26 : 570
  • Kirmse , W. , Baron , W. J. and Seipp , U. 1973 . Angew. Chem. Int. Ed. , 12 : 924
  • Oavis , W. L. , Grunert , R. R. , Hoff , R. F. , McGahem , J. W. , Neumayer , E. M. , Paulshoch , M. , Watts , J. C. , Wood , T. R. , Hermann , E. C. and Hoffmann , C. E. 1964 . Science , 144 : 862
  • Koser , G. F. and Wettach , R. H. 1977 . J. Org. Chem. , 42 : 1476 See also O. Neil and and B. Karele J. Org. Chem., USSR (Engl. Transl.) 1970, 6, 889
  • Chapman , N. B. , Key , J. M. and Toyne , K. J. 1970 . J. Org. Chem. , 35 : 3860
  • Lazbin , I. M. and Koser , G. F. 1987 . J. Org. Chem. , 52 : 476 Ibid, 1986, 51, 2669
  • Della , E. W. , Kasum , B. and Kirkbride , K. P. 1987 . J. Am. Chem. Soc. , 109 : 2746
  • m. p. 105–106°C, IR: vmax 3175 (-CONH-) and 1665 (-CO-NH); 1H NMR (COCl3, OMSO, 200 MHz) δ 7.08–7.67 (m, 9H, C6 H 5, 0-C6 H 4-CH3), 3.92–4.15 (sym, m, 4H, acetal), 3.48–3.68 (m, 5H, homocubyl), 2.95 (m, 1H, C-8), 2.29 (s, 3H, OC6H4-CH 3)
  • Moriarty , R. M. , Khosrowshahi , J. S. and Oalecki , T. M. 1987 . J. Chem. Soc., Chem. Commun. , : 675

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