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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 18, 1988 - Issue 11
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Original Articles

The Preparation of 1-Silyl, β-Allehyl Alcohols, Useful Synthetic Intermediates.

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Pages 1231-1239 | Published online: 06 Dec 2006

References

  • Bertrand , M. , Dulcere , J. P. and Gil , G. 1977 . Tetrahedron Lett. , 43 : 3807
  • Santelli , M. and Bertrand , M. 1973 . Bull. Soc. Chim. , : 2326
  • Weber and William , P. 1983 . Silicon Reagents for Organic Synthesis , 137 New York : Springer-Verlag .
  • Birkofer , L. , Ritter , A. and Uhlenbran , K. H. 1963 . Chem. Ber. , 96 : 3280 1 was prepared in high yields (90X) by monoacetoxylation of the bis-silylacetylen as reported by
  • Kuwajima , I. , TamaKa , T. and Atsumi , K. 1979 . Chem. Lett. , : 779 Hopf, H. in: The Chemistry of Ketenes, Alienes and Related Compounds part. 2 Patai, S., Ed. J. Wiley and Sons, Chichester 1980 p. 784
  • Johnson , A. W. 1966 . Ylid chemistry , Edited by: Blomquist , A. T. 171 – 178 . New York and London : Academic Press .
  • The cis or the trans structure of the olefination products has been deduced by the chemical shift of the C3 vinylic methyl more or less deshielded in agreement with the trans or cis structure of the alkene8
  • Jackman , L. M. and Wiley , R. H. 1960 . J. Chem. Soc. , : 2866
  • The hydralumination of silyl-enynes proceeds almost completely in a trans manner10
  • Eisch , J. J. and Foxton , M. W. 1971 . J. Org. Chem. , 36 : 3520

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