References
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- See reference 2 for an example of a sodium borohydride reduction of a quaternary ammonium salt
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- Infrared spectra were recorded on either a Perkin-Elmer Model 1420 infrared spectrometer as thin films or nujol mulls. NMR spectra were obtained in CCl4, DCCl3, or Me2SO-d6 solutions, (CH3)4 Si internal standard, at 60 MHz with a Varian EM-360 spectrometer., All boiling points and melting points are uncorrected and melting points were recorded on a Fisher-Johns melting-point apparatus. Elemental analyses were carried out by Robertson Laboratory, Inc. of Florham Park, NJ