A Convenient Method for the Large Scale Preparation of (E)-4-Oxo-2-Butenoic Acid Ethyl Ester

References

• Ducher , S. and Michet , A. 1970 . Bull. Soc. Chim. Fr. , : 4353
   Google Scholar
• Veysoglu , T. , Mitscher , L. A. and Swayze , J. K. 1980 . Synthesis , : 807
   Google Scholar
• Witiak , D. T. , Tomita , K. and Patch , R. J. 1981 . J. Med. Chem. , 24 : 788
   PubMed Web of Science ®Google Scholar
• Landor , S. R. , Landor , P. D. and Kalli , M. 1983 . J. Chem. Soc., Perkin Trans. 1 , : 2921
   Google Scholar
• Stotter , P. L. and Eppner , J. B. 1973 . Tetrahedron Lett. , : 2417
   Google Scholar
• Baltes , J. , Stork , L. and Schäfer , H. J. 1979 . Chem. Ber. , 112 : 807
   Google Scholar
• Scharf , H-D. and Janus , J. 1978 . Chem. Ber. , 111 : 2741
   Google Scholar
• Schroeter , S. H. , Appel , R. , Brammer , R. and Schenck , G. D. 1966 . Justus Liebigs Ann. Chem. , 697 : 42
   Google Scholar
• Deshong , P. and Leginus , J. M. 1984 . J. Org. Chem. , 49 : 3421
   Google Scholar
• Stambouli , A. , Amouroux , R. and Chastrette , M. 1987 . Tetrahedron Lett. , : 5301
   Google Scholar
• Mandai , T. , Irei , H. , Kawada , M. and Otera , J. 1984 . Tetrahedron Lett. , : 2371
   Google Scholar
• Ichihara , A. , Ubukata , M. , Oikawa , H. , Marakami , K. and Sakamura , S. 1980 . Tetrahedron Lett. , : 4469
   Google Scholar
• Corey , E. J. and Molnet , G. 1973 . Amer. Chem. Soc. , 95 : 7185
   PubMed Web of Science ®Google Scholar
• Trippett , S. and Walker , D. M. 1961 . J. Chem. Soc. , : 1266 or commercial sources such as Aldrich Chemical Co.
   Web of Science ®Google Scholar
• Carlo Erba FV 4160: J&W DB-5 column, 15M x 0.32mm, film thickness of 0.25μ, in split mode at 60°C isothermal, using He at 3 ml min−1
   Google Scholar
• A similar reaction gave an oil in 78% yield, with 96% purity by G. C., suitable for use without further purification
   Google Scholar
• Bruker AM 250
   Google Scholar