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- TLC analysis (light petroleum/ethyl acetate 70/30) showed the complete disappearance of the starting material. Mass spectra were in agreement with the transformation of compounds 3 and 9 into the corresponding sulfoxides (m/z: 276, 260, 151, 135, 107, 91 and 344, 328, 219, 191, 203, 175, 109, 91 respectively).