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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 20, 1990 - Issue 11
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Original Articles

Formal Total Synthesis of Ipomeamarone via the [2+3] Dihydrofuran Annulation

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Pages 1721-1732 | Received 21 Mar 1990, Published online: 24 Oct 2006

References

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  • Ratio determined by NMR/GC. All compunds gave satisfactory 1H and 13C-NMR as well as mass spectral data consistent with their structures .
  • Hudlicky , T. , Sinai-Zingde , G. and Natchus , M. G. 1987 . Tetrahedron Lett. , 28 : 5287 I.K. Youn, G. H. Yon, C.S. Pak, Tetrahedron Lett. 198627, 2409
  • The presence of hydroxy absorption in the IR of 9 was originally misinterpreted as hydrate of 10a,b accounting for the erroneous analytical results. (All other spectral data (1H-NMR, 13C-NMR, GC/MS) were consistent with structures 10a,b

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