Preparation and Reaction of Cyclic Oxalate of Diols

References

• Markiewicz , W. T. 1979 . J. Chem. Res. Synop. , : 24
   Web of Science ®Google Scholar
• Hough , L. , Priddle , J. E. and Theobald , R. S. 1960 . Adv. Carbohydr. Chem. , 15 : 91
   PubMedGoogle Scholar
• Amarnath , V. and Broom , A. D. 1977 . Chem. Rev. , 77 : 183
   Web of Science ®Google Scholar
• Wilkinson , S. G. 1979 . “Comprehensive Organic Chemistry,” , Edited by: Stoddart , J. F. Vol 1 , 679 New York : Pergamon Press .
   Google Scholar
• Davies , A. G. , Hua-De , P. and Hawari , J. A. 1983 . J. Organomet. Chem. , 256 : 251
   Google Scholar
• Compound 7; TLC (SiO2, ether) Rf = 0.70; mp 143–144°C; IR (KBr) 2980, 1790, 1760 cm−1; 1H NMR (CDCl3) δ1.36 (s, 6H), 1.97 (s, 6H), 4.0–4.5(m, 8H)
   Google Scholar
• Compound 10; TLC (SiO2, ether) Rf = 0.74; IR (KBr) 2980, 1760, 1740 cm–1; 1H NMR (CDCl3); δ1.2 (m, 18H, CH3), 3.8–4.4 (m, 10H) 5.2–5.5 (dd, 2H)
   Google Scholar
• Fersht , A. R. and Jencks , W. P. 1970 . J. Amer. Chem. Soc. , 92 : 5432 5442
   Web of Science ®Google Scholar
• Compound 13; TLC (SiO2, 8:2 chloroform/methanol) Rf = 0.23; mp 180–181°C; IR (KBr) 3400, 1780 cm−1; 1H NMR (DMSO-d6) δ3.4–3.7 (m, 6H), 3.7–4.2(m, 2H)
   Google Scholar
• Financial support from the Korea Science and Engineering Foundation and the Organic Chemistry Research Center is gratefully acknowledged
   Google Scholar