The Preparation of Thiol Formates

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• Jaenicke and Koch, Ref. 3b. They state that 1 (prepared from formyl fluoride) quickly liquifies in air and decomposes. Their product must have been contaminated since we have found 1 to be stable even on four months' exposure to air at ambient temperatures, but to have mostly hydrolyzed and partially rearranged after 29 years in refrigerator.
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• Decoupling showed that the two narrow multiplets are due to long range coupling of the X2AA ‘BB’ system with 1/2(4J + 5J) = 0.5 ± 0.1 Hz.
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