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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 22, 1992 - Issue 20
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Original Articles

The Preparation of Thiol Formates

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Pages 2949-2954 | Received 04 Jun 1992, Published online: 23 Sep 2006

References

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  • This compound was prepared by M.S. by the method described, in the laboratory of D.B. Sprinson, Department of Biochemistry, College of Physicians and Surgeons, Columbia University, N.Y., in Sept. 1963.
  • Jaenicke and Koch, Ref. 3b. They state that 1 (prepared from formyl fluoride) quickly liquifies in air and decomposes. Their product must have been contaminated since we have found 1 to be stable even on four months' exposure to air at ambient temperatures, but to have mostly hydrolyzed and partially rearranged after 29 years in refrigerator.
  • Decoupling showed that the two narrow multiplets are due to long range coupling of the X2AA ‘BB’ system with 1/2(4J + 5J) = 0.5 ± 0.1 Hz.

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