References
- Caracas, , Venezuela : Central University of . On leave from the School of Chemistry
- Montanari , F. 1956 . Gazz. Chim. Ital , 86 : 735
- Parham , W. E. and Stright , P. L. 1956 . J. Am. Chem. Soc. , 78 : 4783
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- Dehmlow , E. V. and Lissel , M. 1981 . Tetrahedron , 37 : 1653
- Lipshutz , B. H. and Ellsworth , E. L. 1990 . J. Am. Chem. Soc. , 112 : 7440
- Babiak , K. A. , Behling , J. R. , Dygos , J. H. , Mclaughlin , K. T. , Ng , J. S. , Kalish , V. J. , Kramer , S. W. and Shone , R. L. 1990 . J. Am. Chem. Soc. , 112 : 7441
- Bondi , A. J. 1964 . Phys. Chem. , 68 : 441
- The distillation must be performed at <50°C to avoid loss of product by elimination of HCl
- The receiving vessel should be cooled to -10°C
- The chloroethyl thioether is stable for several months at -5°C
- The receiving vessel should be cooled to -30°C
- The ethynyl sulfide is stable for at least 8 months if stored at -20°C in the absence of oxygen