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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 22, 1992 - Issue 10
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Original Articles

A New Synthesis of 2′,3′-Dideoxyinosine

V. Bhat Pharm-Eco Laboratories, Inc., 2355 Chain Drive, Simi Valley, California, 93065, U.S.A.; Calbiochem Corporation, 10933 North Torrey Pines Road, La Jolla, CA, 92037
,
E. Stocker Pharm-Eco Laboratories, Inc., 2355 Chain Drive, Simi Valley, California, 93065, U.S.A.
&
B. G. Ugarkar Pharm-Eco Laboratories, Inc., 2355 Chain Drive, Simi Valley, California, 93065, U.S.A.; Gensia Pharmaceuticals, Inc., 11075 Roselle St., San Diego, CA, 92121-1207
Pages 1481-1486 | Received 10 Jan 1992, Published online: 23 Sep 2006

References

  • Current address: Calbiochem Corporation, 10933 North Torrey Pines Road, La Jolla, CA 92037
  • Current address: Gensia Pharmaceuticals, Inc., 11075 Roselle St., San Diego, CA 92121–1207
  • Dagani , R. 1987 . Chem. Eng. News , 20 : 41
  • Mitsuya , H. and Broder , S. 1986 . Proc. Natl. Acad. Sci. USA , 83 : 1911
  • Beach , C. M. , Evans , R. K. and Coleman , M. S. 1991 . Nucleosides & Nucleotides , 10 : 1499 and the references cited therein
  • Chu , C. K. , Bhadti , V. S. , Doboszewski , B. , Gu , Z. P. , Kosugi , Y. , Pullaiah , K. C. and Roey , P. V. 1989 . J. Org. Chem. , 54 : 2217
  • Robins , M. J. , Hansske , F. , Low , N. H. and Park , J. I. 1984 . Tetrahedron Lett. , 25 : 367
  • Addition of acetic acid is not necessary if the Zn/Cu couple is fresh
  • The organic layer was washed more, if necessary, with 10% aqueous EDTA trisodium salt solution until it gives a clear solution with aqueous NaHCO3

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