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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 23, 1993 - Issue 4
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Original Articles

An Improved Procedure for α-Methylenation of Lactones

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Pages 495-503 | Received 02 Sep 1992, Published online: 23 Sep 2006

References

  • Grieco , P. A. 1975 . Synthesis , : 67 – 82 . For reviews on the synthesis of α-methylene-γ-butyrolactones, see: (a)
  • Hoffmann , H. M. R. and Rabe , J. 1985 . Angew. Chem. Int. Ed. Engl. , 24 : 94 – 110 .
  • Petragnani , N. , Ferraz , H. M. C. and Silva , G. V. J. 1986 . Synthesis , : 157 – 183 .
  • Murta , M. M , de Azevedo , B. M. M. and Greene , A. E. 1992 . J. Org. Chem. , 57 : 4567 – 4569 .
  • Cavallito , C. J. , Fruehauf , McK. D. and Bailey , J. N. 1948 . J. Am. Chem. Soc. , 70 : 3724 – 3726 .
  • Van Tamelen , E. E. and Bach , S. R. 1958 . J. Am. Chem. Soc. , 80 : 3079 – 3086 .
  • Martin , J. , Watts , P. C. and Johnson , F. 1974 . J. Org. Chem. , 39 : 1676 – 1681 .
  • Carlson , R. M. and Oyler , A. R. 1976 . J. Org. Chem. , 41 : 4065 – 4069 .
  • Martin , J. , Watts , P. C. and Johnson , F. 1970 . J. Chem. Soc., Chem. Commun. , : 27
  • Stiles , M. 1959 . J. Am. Chem. Soc. , 81 : 2598 – 2599 .
  • Finkbeiner , H. and Stiles , M. 1963 . J. Am. Chem. Soc. , 85 : 616 – 622 . The methyl methoxymagnesium carbonate (MMC) used in this work was purchased from Aldrich
  • Gras , J.-L. 1978 . Tetrahedron Lett. , : 2111 – 2114 .
  • 1979 . Aldrichimica Acta , 12 ( 1 ) : 20 N-Methylanilinium trifluoroacetate with paraformaldehyde in refluxing THF or dioxane has been used for α-methylenation of ketones. See
  • Grieco , P. and Hiroi , K. 1973 . J. Chem. Soc., Chem. Commun. , : 500 – 501 .
  • Corey , E. J. and Ravindranathan , T. 1971 . Tetrahedron Lett. , : 4753 – 4755 .
  • Carlson , R. M. and White , L. L. 1983 . Synth. Commun. , 13 : 237 – 241 .
  • Stetter , H. and Marten , K. 1982 . Liebigs Ann. Chem. , : 240 – 249 .

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