Stereoselective Synthesis of An Isoquinolinopyrrolidinone by Acyliminium Ion Cyclization of Chiral Hydroxylactams

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• Crystal data for 3 were collected with use of Enraf-Nonius CAD4 automated diffractometer equipped with a Mo X-ray rub and graphite crystal monochromator: C12H13O3N, orthorhombic, space group P212121, α=8.205(5), β=10.229(2), γ=13.277(3) Å, V=1114.4(8) Å3, Z=4, dcalc=1.295g cm−3, the final R value is 0.060 for 526 reflections with 3°<2θ<50°.
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