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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 25, 1995 - Issue 13
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Original Articles

Dialkylborane-Catalyzed Hydroboration of Alkynes with 1,3,2-Benzodioxaborole in Tetrahydrofuran

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Pages 1957-1962 | Received 24 Aug 1994, Published online: 23 Sep 2006

References

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  • Pelter , A. , Smith , K. and Brown , H. C. 1988 . Borane Reagents , London : Academic Press . For example
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  • Kabalka , G. W. , Narayama , C. and Reddy , N. K. 1994 . Synth. Commun. , 24 : 1019
  • For example, see literatures cited in ref. 4 (b).
  • Suseela , Y. , Prasad , A. S. B. and Periasamy , M. 1990 . J. Chem. Soc., Chem. Commun. , : 446
  • 1H NMR (CDCl3, TMS) d=0.92 (t, J=7 Hz, 3H), 1.1–1.7 (m, 4H), 2.15–2.4 (m, 2H), 5.78 (dt, J=18 and 1.5 Hz, 1H), and 6.9–7.3 (m, 5H).
  • Brown , H. C. , Hamaoka , T. and Ravindran , N. 1973 . J. Am. Chem. Soc. , 95 : 5786 A known method for the replacement of the boronic acid moiety by iodine with retention of configuration
  • Brown , H. C. , Hamaoka , T. , Ravindran , N. , Subrahmanyam , C. , Somayaji , V. and Bhat , N. G. 1989 . J. Org. Chem. , 54 : 6075
  • Miyaura , N. and Suzuki , A. 1979 . J. Chem. Soc., Chem. Commun. , : 866 A known method for the replacement of the 1,3,2-benzodioxaboryl group by phenyl group with retention of configuration
  • Zweifel , G. , Clark , G. M. and Polston , N. L. 1971 . J. Am. Chem. Soc. , 93 : 3395
  • Brown , H. C. , Scouten , C. G. and Liotta , R. 1979 . J. Am. Chem. Soc. , 101 : 96

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