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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 26, 1996 - Issue 21
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Original Articles

A Practical Synthesis of SDZ WAG 994 by Selective Methylation of N6-Cyclohexyladenosine

Mahavir Prashad Chemical Research & Development, Technical R & D Sandoz Reasearch Institute Sandoz Pharmaceuticals Corporation, 59 Route 10, East Hanover, NJ, 07936
,
Kapa Prasad Chemical Research & Development, Technical R & D Sandoz Reasearch Institute Sandoz Pharmaceuticals Corporation, 59 Route 10, East Hanover, NJ, 07936
&
Oljan Repic Chemical Research & Development, Technical R & D Sandoz Reasearch Institute Sandoz Pharmaceuticals Corporation, 59 Route 10, East Hanover, NJ, 07936
Pages 3967-3977 | Received 19 May 1996, Published online: 23 Aug 2006

References

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  • Yamada , T. and Kageyama , K. EP 0 378 518 A2 . January 11 1990 .
  • Chemical R & D , Basel, , Switzerland : Sandoz Ltd. . Unpublished results
  • Robins , M. J. , Naik , S. R. and Lee , A. S. K. 1974 . J. Org. Chem. , 39 : 1891
  • Yamauchi , K. , Nakagima , T. and Kinoshita , M. 1986 . Bull. Chem. Soc. Jpn. , 59 : 2947
  • Kazimierczak , Z. , Darzynkiewicz , E. and Shugar , D. 1976 . Biochemistry , 15 : 2735
  • Gadient , F. DE 4039060 A1 . June 11 1992 .
  • “ 6-Chloro-9-(2′,3′,5′-tri-O-acetyl-β-D-ribofuranosyl)-9H-purine, described in reference 2a, was treated with cyclohexylamine to furnish pure N6-cyclohexyladenosine (unpublished results ” . In Chemical R & D , Basel : Sandoz Ltd. .
  • Fleysher , M. H. 1972 . J. Med. Chem. , 15 : 187
  • Prashad , M. , Prasad , K. and Repic , O. 1994 . Nucleosides & Nucleotides , 13 : 945

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