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- Significantly, the 1:2 bromine:2-naphthoxide stoichiometry employed in the novel procedure suppresses effectively the formation of higher brominated by-products arising in the preparation of 1-bromo-2-naphthol by a routine bromination
- Concurrently with the dominant (95%) cross-coupling between 1a and 2a, a minor self-coupling reaction of 2a takes place (ref.6). In order to achieve a complete conversion of 1a in the overall reaction, it is accordingly recommended to increase the calculated amount of bromine by about 10%
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