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- The coupling constant (J 112,113=0 Hz) between 2-H and 3-H in 1H NMR (JEOL GX-270) of 2-phenyl-3-vinyltetrahydrofuran (5; R=Ph) suggested that the stereochemistry in a major isomer of all 2-substituted 3-vinyltetrahydrofurans 5 was trans (cis:trans=1:9).
- Cyclic carbonate of 4-hexene-1,3-diol, namely 4-[(E)-2-propenyl]-1,3-dioxan-2-one caused the carbonyl allylation at room temperature neither in DMF nor in THF.