A Convenient Synthesis of 3-Aryl-3-(5,5-dimethyl-3-hydroxy-2-cyclohexene-1-one-2-yl) Propanic Esters Catalyzed by KF-Alumina

Daqing Shi Department of Chemistry, Xuzhou Normal University, Xuzhou, 221009, P. R. China

Shujiang Tu Department of Chemistry, Xuzhou Normal University, Xuzhou, 221009, P. R. China

Zaisheng Lu Department of Chemistry, Xuzhou Normal University, Xuzhou, 221009, P. R. China

Suhui Wang Department of Chemistry, Xuzhou Normal University, Xuzhou, 221009, P. R. China

Guiyuan Dai Department of Chemistry, Xuzhou Normal University, Xuzhou, 221009, P. R. China

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X-ray analysis of 4a: Empirical formula C18H21ClO4, F.W. 336.81, T=293K, monoclinic, space group P21/a, a=7.587(2)Å, b=11.736(3)Å, c=19.120(7)Å, β=101.30(3)Å, V=1669.5(9)Å3, Z=4, Dc =1.340 g · cm−3, F(000) =712, λ(MoKα)=0.71069Å, μ=2.46cm−1, 6°<2θ<50.0°, R=0.034, Rw=0.042. largest diff. peak 0.18e · Å−3.
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A Convenient Synthesis of 3-Aryl-3-(5,5-dimethyl-3-hydroxy-2-cyclohexene-1-one-2-yl) Propanic Esters Catalyzed by KF-Alumina

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A Convenient Synthesis of 3-Aryl-3-(5,5-dimethyl-3-hydroxy-2-cyclohexene-1-one-2-yl) Propanic Esters Catalyzed by KF-Alumina

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