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- Silica gel (100–200 mesh) was used for column chromatography with petroleum ether/ethyl acetate as eluant. IR spectra were recorded with a Perkin‐Elmer 681 spectrometer. NMR spectra were recorded at 60 MHz (CW, EM 360, Varian and FT, Hitachi‐R‐600), 500 MHz (Bruker, AM‐500) in CDCI3 using TMS as internal standard, J values are given in Hz. Mass spectra were recorded with Shimadzu MS‐QP 1000 spectrometer at 70 ev