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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 29, 1999 - Issue 8
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Original Articles

Chlorine Substitution Reactions using Trichloroisocyanuric Acid with Triphenylphosphine

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Pages 1415-1419 | Received 13 Oct 1998, Published online: 17 Sep 2007

References

  • Larock , R. C. 1989 . Comprehensive Organic Transformations , New York : VCH Publishers . For references to all of the reactions mentioned see
  • Hiegel , G. A. , Bayne , C. D. , Donde , Y. , Tamashiro , G. S. and Hilberath , L. A. 1996 . Synth. Commun. , 26 ( 14 ) : 2633 and references cited therein
  • The acid chloride was converted into the methyl ester before isolation
  • Eaton , E. 1964 . Mfg. Chemist and Aerosol News , 35 ( 12 ) : 45 TCICA is reported to be about 88% reactive as determined by a thiosulfate titration of the iodine liberated on reaction with iodide so a slight excess was used. See
  • The IR of the solid matched that of cyanuric acid (C3H3O3N3)
  • Piers , E. , Grierson , J. R. , Lau , C. K. and Nagakura , I. 1982 . Can. J. Chem. , 60 : 210

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