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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 29, 1999 - Issue 14
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Original Articles

BoC2O Mediated Macrolactonisation: Syntheses of R-(+)-Ricinoleic Acid Lactone and (±)-12-OH-Stearic Acid Lactone

Pages 2467-2475 | Received 19 Dec 1998, Published online: 17 Sep 2007

References

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  • The stereochemistry and enantiomeric excess of acetate 4 was determined from the optical rotation of the target lactone 1, [α]D +30.49 (c,0.94,CHCl3 lit6g [α]D +32.2 (c,1.0,CHCl3), from which the %ee was ascertained to be 94.6

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