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Original Articles

A Convenient Preparation of Trimethylborane and Triethylborane

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Pages 359-367 | Received 01 Feb 1973, Accepted 29 May 1973, Published online: 06 Dec 2006

References

  • Grassberger , M. 1971 . Organische Borverbindungen , Weinheim/Bergstr : Verlag Chemie . Chemische Taschenbücher 15
  • Köster , R. , Amen , K.-L. , Bellut , H. and Fenzl , W. 1971 . Angew. Chemie , 83 : 805 Angew. Chem. internat. Edit 10, 748 (1971
  • Brown , H. C. 1945 . J. Amer. Chem. Soc. , 67 : 374
  • Frankland , E. 1862 . Liebigs Annalen Chem. , 124 : 129
  • Stock , A. and Zeidler , F. 1921 . Ber. dtsch. chem. Ges. , 54 : 531
  • Köster , R. 1958 . Liebigs Ann. Chem. , 618 : 31
  • Nöth , H. and Storch , W. 1971 . Synthesis in Inorganic and Metal-Organic Chemistry , 1 : 197
  • Wiberg , E. , Hertwig , K. and Goubeau , J. 1949 . FIAT Review of German Science , Vol. 23 , 228 Wiesbaden : Dieterich'sche Verlagsbuch-handlung .
  • Barnes , R. L. and Wartik , T. 1963 . J. Amer. Chem. Soc. , 85 : 360
  • Casanova , J. Jr. , Kiefer , H. R. and Williams , R. E. 1969 . Organic Preparations and Procedures , 1 : 57
  • Brit. Pat. . 768765 . 10. 2. 1957 . Kalichemie AG Hannover; C. A. 52, 421 (1958)
  • Prepared from aluminum powder and MeCl11 or purchased from Texas Alkyls Div. , Deer Park, Texas : Stauffer Chemicals Co. . 77536
  • Lehmkuhl , H. and Ziegler , K. 1970 . Houben-Weyl Bd. , Vol. 13/4 , 63 Georg Thieme Verlag Stuttgart .
  • Prepared from B2O3 and n-BuOH13 or purchased from Eastman Organic Chemicals.
  • Johnson , J. R. and Tompkins , S. W. 1943 . Org. Synth. Coll. Vol. , 2 : 106
  • Köster , R. 1963 . Houben-Weyl , Vol. 6/2 , 194 Stuttgart : Georg Thieme Verlag .
  • Et3Al is available from Schering AG, Bergkamen/Westfalen, Germany or Texas Alkyls Div., Stauffer Chemical Co., Deer Park, Texas 77536.
  • Et2O[sbnd]BF3 is (B. P. 50° at 15 torr) available from BASF AG, Ludwigshafen/Rhein, Germany or Eastman Organic Chemicals.
  • Riedel-de-Haen , A G. Seelze bei Hannover , Beverly, Mass : Germany or Ventron Corp. . 01915, P. O. Box 159
  • A mixture of saturated hydrocarbons with b. p. 190° from Esso AG, Hamburg, Germany.

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