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Original Articles

Synthesis of Cr(iii) Porphyrin Complexes and Their 51Cr Labeled Congeners

Pages 147-161 | Received 19 Sep 1979, Accepted 19 Nov 1979, Published online: 03 Jan 2007

References

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  • Mertz , W. and Cor'natzer , W. , eds. 1971 . “ chapts. 7–9 ” . In Newer Trace Elements In Nutrition , 125 – 193 . New York : Marcel Dekker .
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  • Schroeder , H. A. , Balassa , J. J. and Tipton , I. H. 1962 . J. Chromic Diseases , 15 : 941
  • Cr(III) complexes are used because the 3 oxidation state is the only one that will exist in living systems
  • Tsutsui , M. , Ichikawa , M. , Vohwinkel , F. and Suzuki , K. 1966 . J. Amer. Chem. Soc. , 88 : 854
  • Tsutsui , M. , Velapoldi , R. A. , Suzuki , K. , Vohwinkel , F. , Ichikawa , J. and Koyano , T. 1969 . J. Amer. Chem. Soc. , 9.1 : 6262
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  • The Cr porphyrin synthetic route of ref. 9 utilizes Cr(II)Cl 2as the starting material, but the reaction is done in the air; consequently, much of the Cr(II) is oxidized to the inert Cr(III) state before incorporation. This requires that an excess of Cr(II) be used to insure complete porphyrin consumption
  • McLendon , G. and Baily , M. 1979 . Inorg. Chem. , JL8 ( 8 ) : 2120
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  • Chap. 5 190 Reference 12
  • This activity level is necessary to give good counting statistics in a whole body counter when about 1% of a dose of 5 yg of Cr is absorbed by a rat
  • Adler , A. , Longo , F. R. , Finaralli , J. D. , Goldmacher , J. , Assour , J. and Korsakoff , L. 1967 . J. Org. Chem. , 32 : 476
  • Adler , A. D. , Sklar , L. , Longo , F. R. , Finarelli , J. D. and Finarelli , M. G. 1968 . J. Heterocycl. Chem. , 5 : 669
  • Fleischer , E. B. , Palmer , J. M. , Srivastava , T. S. and Chatterjee , A. 1971 . J. Amer. Chem. Soc. , 93 ( 13 ) : 3163
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  • 1975 . Chap. 19 , 834 – 5 . Published by Elsevier . Reference 12
  • The two resins were Dowex 50W-X8 (20–50 mesh) and Baker CGC-241
  • Fleischer , E. B. and Krishnamurthy , M. 1972 . J. Coord. Chem. , 2 : 89 – 100 .

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