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- Continued bubbling after initial saturation leads to the formation of tarry residues. This is more apparent using α-hydroxethyl ferrocenes
- A chilled sample of neat dimethylamine was used in this preparation, however, satisfactory results may be achieved using a 40% aqueous solution of dimethylamine
- When an aqueous solution of the amine was used no precipitate was observed. The benzene solution was separated, dried over anhydrous MgSO4, and its solvent volume reduced to a few mLs. prior to column chromatography. Product yields were not diminished when aqueous amines were used
- Oil crystallised on standing for 1–2 weeks