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Original Articles

Determination of fluoroquinolones in aquaculture products by ultra-performance liquid chromatography-tandem mass spectrometry (UPLC-MS/MS)

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Pages 39-46 | Received 16 Jan 2008, Accepted 07 May 2008, Published online: 07 Oct 2010

References

  • AOAC . 2000 . “ AOAC official methods of analysis ” . In . Method 937-07 Fish and marine products–treatment and sample preparation procedure , 17th Edn , Gaithersburg, MD : AOAC International . sect. 35.1.01
  • Bethem , R , Boison , JO , Gale , J , Heller , D , Lehotay , S , Loo , J , Musser , S , Price , P and Stein , S . 2003 . Establishing the fitness for purpose of mass spectrometric methods . J Am Soc Mass Spectrom , 14 : 528 – 541 .
  • Canadian Food Inspection Agency . 2005 . “ Fish products standards and methods manual ” . In Approved theraputants for aquaculture use , Ottawa, ON(Canada) : Canadian Food Inspection Agency . Appendix No. 1 2005
  • Dufresne , G and Fouquet , A . 2007 . Multiresidue determination of quinolone and fluoroquinolone antibiotics in fish and shrimp by liquid chromatography/tandem mass spectrometry . J AOAC Int , 90 : 604 – 612 .
  • EURACHEM guide. The fitness for purpose of analytical methods: a laboratory guide to method validation and related topics. Eurachem Working Group Report, December 1998 , EURACHEM. 1998
  • European Communities Commission Decision (ECCD) . 2002 . Implementing Council Directive 96/23/EC concerning the performance of analytical methods and the interpretation of results . Off J Eur Comm , L221 : 8 – 36 .
  • Kowalczuk , D , Hopkala , H and Gumieniczek , A . 2003 . Application of solid-phase extraction of fluoroquinolone derivatives from a biological matrix to their biodetermination by liquid chromatography . J Liq Chromatog Relat Tech , 26 : 1731 – 1741 .
  • McNabb , P , Selwood , AI and Holland , PT . 2005 . Multiresidue method for determination of algal toxins in shellfish: single-laboratory validation and interlaboratory study . J AOAC Int , 88 : 761 – 772 .
  • Pecorelli , I , Galarini , R , Bibi , R , Floridi , AL , Casciarri , E and Floridi , A . 2003 . Simultaneous determination of 13 quinolones from feeds using accelerated solvent extraction and liquid chromatography . Anal Chimica Acta , 483 : 81 – 89 .
  • Roybal , JE , Pfenning , AP , Turnipseed , SB , Walker , CC and Hurlbut , JA . 1997 . Determination of four fluoroquinolones in milk by liquid chromatography . J AOAC Int , 80 : 982 – 987 .
  • Roybal , JE , Walker , CC , Pfenning , AP , Turnipseed , SB , Storey , JM , Gonzales , SA and Hurlbut , JA . 2003 . Concurrent determination of four fluoroquinolones in catfish, shrimp and salmon by LC with fluorescence detection . J AOAC Int , 85 : 1293 – 1301 .
  • Samanidou , VF , Demetriou , CE and Papadoyannis , IN . 2003 . Direct determination of four fluoroquinolones; enozacin, norfloxacin, ofloxacin and ciprofloxacin, in pharmaceuticals and blood serum by HPLC . Anal Bioannal Chem , 375 : 623 – 629 .
  • Schneider , MJ , Darwish , AM and Freeman , DW . 2007 . Simultaneous multiresidue determination of tetracyclines and fluoroquinolones in catfish muscle using high performance liquid chromatography with fluorescence detection . Anal Chemica Acta. , 586 : 269 – 274 .
  • Schneider , MJ and Donoghue , DJ . 2003 . Multiresidue determination of fluoroquinolone antibiotics in eggs using liquid chromatography-fluorescence-mass spectrometry . Anal Chimica Acta , 483 : 39 – 49 .
  • Steffenak , I , Hormazabal , V and Yndestad , M . 1991 . A rapid assay for the determination of sarafloxacin (A-55620) in fish by high performance liquid chromatography . J Liq Chrom , 14 : 1983 – 1989 .
  • Tittlemier , SA , Van de Riet , JM , Burns , G , Potter , R , Murphy , C , Rourke , W , Pearce , H and Dufresne , G . 2007 . Analysis of veterinary drug residues in fish and shrimp composites collected during the Canadian Total Diet Study, 1993–2004 . Food Add. Contam , 24 : 14 – 20 .
  • Toussaint , B , Bordin , G , Janosi , A and Rodriguez , AR . 2002 . Validation of a liquid chromatography-tandem mass spectrometry method for the simultaneous quantification of 11 fluoroquinolone antibiotics in swine kidney . J Chromatog A , 976 : 195 – 206 .
  • Turnipseed , SB , Roybal , JE and Pfenning , AP . 2006 . Confirmation of fluoroquinolone residues in salmon and shrimp tissue by LC/MS: evaluation of single quadrapole and ion trap instruments . USFDA Lab Informat Bull , 4298 : 1 – 20 .
  • US Food and Drug Administration . 2005 . Guidance for industry: mass spectrometry for confirmation of the identity of animal drug residues , Washington, DC : US Food and Drug Administration . [cited 2005 Jan 20]. Available from: http://www.fda.gov/cvm/guidance/guide118.doc/
  • van de Riet , JM , Murphy , CJ , Pearce , JN , Potter , RA and Burns , BG . 2005 . Determination of malachite green and leucomalachite green in a variety of aquacultured products by liquid chromatography with tandem mass spectrometry detection . J AOAC Int , 88 : 744 – 749 .

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