134
Views
6
CrossRef citations to date
0
Altmetric
Original Articles

Confirmatory method for the determination of various acetylgestagens in animal kidney fat using liquid chromatography–tandem mass spectrometry

, , , &
Pages 672-682 | Received 16 Sep 2008, Accepted 22 Nov 2008, Published online: 24 Jun 2009

References

  • Commission Decision 2002/657/EC. Commission Decision 2002/657/EC of 12 August 2002 implementing Council Directive 96/23/EC concerning the performance of analytical methods and the interpretation of results. Off J Eur Commun. L2218
  • Commission Decision 2003/181/EC. Commission Decision 2003/181/EC of 13 March 2003 amending Decision 2002/657/EC as regards the setting of minimum required performance limits (MRPLs) for certain residues in food of animal origin. Off J Eur Commun. L7117
  • Council Directive 96/22/EC . 1996 . Concerning the prohibition on the use in stockfarming of certain substances having a hormonal or thyrostatic action and of ß-agonists . Off J Eur Commun , L125
  • Council Directive 96/23/EC . 1996 . On measures to monitor certain substances and residues thereof in live animals and animal products . Off J Eur Commun , L221
  • CRL Guidance Paper. 2007. CRLs view on state of the art analytical methods for national residue control plans; 7 December 2007. Community Reference Laboratory, RIVM, Bilthoven, The Netherlands
  • Daeseleire , E , Vanoosthuyze , K and Van Peteghem , C . 1994 . Application of high-performance thin-layer chromatography and gas chromatography–mass spectrometry to the detection of new anabolic steroids used as growth promotors in cattle fattening . J Chromatogr A , 674 : 247 – 253 .
  • Daeseleire , E , Vandeputte , R and Van Peteghem , C . 1998 . Validation of multi-residue methods for the detection of anabolic steroids by GC–MS in muscle tissues and urine samples from cattle . Analyst , 123 : 2595 – 2598 .
  • Daxenberger , A , Meyer , K , Hageleit , M and Meyer , HHD . 1999 . Detection of melengestrol acetate residues in plasma and edible tissues of heifers . Vet Q , 21 : 154 – 157 .
  • Hageleit , M , Daxenberger , A and Meyer , HHD . 2001 . A sensitive enzyme immunoassay (EIA) for the determination of melengestrol acetate (MGA) in adipose and muscle tissues . Food Addit Contam , 18 : 285 – 291 .
  • Hooijerink , H , van Bennekom , EO and Nielen , MWF . 2003 . Screening for gestagens in kidney fat using accelerated solvent extraction and liquid chromatography electrospray tandem mass spectrometry . Anal Chim Acta , 483 : 51 – 59 .
  • Impens , S , De Wasch , K , Cornelius , M and De Brabander , HF . 2002 . Analysis on residues of estrogens, gestagens and androgens in kidney fat and meat with gas chromatography–tandem mass spectrometry . J Chromatogr A , 970 : 235 – 247 .
  • Impens , S , Courtheyn , D and De Wasch , K . 2003 . Faster analysis of anabolic steroids in kidney fat by downscaling the sample size and using gas chromatography–tandem mass spectrometry . Anal Chim Acta , 483 : 269 – 280 .
  • ISO/IEC 17025 2005. General requirements for the competence of testing and calibration laboratories. International Organization for Standardization 2005
  • Krzeminski , LF , Cox , BL and Gosline , RE . 1981 . Fate of radioactive melengestrol acetate in the bovine . J Agric Food Chem , 29 : 387 – 391 .
  • Lohmus , M and Kender , T . 2007 . Determination of gestagens in kidney fat by liquid chromatography–tandem mass spectrometry . Anal Chim Acta , 586 : 233 – 238 .
  • Marchand , P , Le Bizec , B , Gade , C , Monteau , F and Andre , F . 2000 . Ultra trace detection of a wide range of anabolic steroids in meat by gas chromatography coupled to mass spectrometry . J Chromatogr A , 867 : 219 – 233 .
  • Mortensen , SK and Pedersen , M . 2007 . Confirmatory analysis of acetylgestagens in plasma using liquid chromatography–tandem mass spectrometry . Anal Chim Acta , 586 : 217 – 222 .
  • Rambaud , L , Bichon , E , Cesbron , N , Andre , F and Le Bizec , B . 2005 . Study of 17-estradiol-3-benzoate, 17-methyltestosterone and medroxyprogesterone acetate fixation in bovine hair . Anal Chim Acta , 532 : 165 – 176 .
  • Rapp , M and Meyer , HHD . 1989 . Control of illegal medroxyprogesterone acetate: application in veal calves by residue analysis in adipose tissues using HPLC/RIA method . Food Addit Contam , 6 : 59 – 70 .
  • Rosen , J , Hellenas , KE , Tornqvist , P and Shearan , P . 1994 . Automated extraction of acetylgestagens from kidney fat by matrix solid phase dispersion . Analyst , 119 : 2635 – 2638 .
  • SANCO/2004/2726rev1 2004. Guidelines for the implementation of Commission Decision 2002/657/EC
  • Stolker , AAM , Zoontjes , PW and van Ginkel , LA . 1998 . The use of supercritical fluid extraction for the determination of steroids in animal tissues . Analyst , 123 : 2671 – 2676 .
  • Stolker , AAM , Zoontjes , PW , Schwillens , PLWJ , Kootstra , PR , van Ginkel , LA , Stephany , RW and Brinkman , UATh . 2002 . Determination of acetyl gestagenic steroids in kidney fat by automated supercritical fluid extraction and liquid chromatography ion-trap mass spectrometry . Analyst , 127 : 748 – 754 .
  • Vanoosthuyze , K , Daeseleire , E , Van Overbeke , A and Van Peteghem , C . 1994 . Survey of the hormones used in cattle fattening based on the analysis of Belgian injection sites . Analyst , 119 : 2655 – 2658 .

Reprints and Corporate Permissions

Please note: Selecting permissions does not provide access to the full text of the article, please see our help page How do I view content?

To request a reprint or corporate permissions for this article, please click on the relevant link below:

Academic Permissions

Please note: Selecting permissions does not provide access to the full text of the article, please see our help page How do I view content?

Obtain permissions instantly via Rightslink by clicking on the button below:

If you are unable to obtain permissions via Rightslink, please complete and submit this Permissions form. For more information, please visit our Permissions help page.