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Food Additives & Contaminants: Part A Volume 26, 2009 - Issue 11
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Original Articles

Validation of a liquid chromatography-tandem mass spectrometry screening method to monitor 58 antibiotics in milk: a qualitative approach

M. Gaugain-Juhel Community Reference Laboratory for Antimicrobial Residues, Agence Française de Sécurité Sanitaire des Aliments, Laboratoire d’Etude et de Recherche sur les Médicaments Vétérinaires et les Désinfectants, La Haute-Marche, BP90203, F-35302 Fougères Cedex, FranceCorrespondence[email protected]
,
B. Delépine Community Reference Laboratory for Antimicrobial Residues, Agence Française de Sécurité Sanitaire des Aliments, Laboratoire d’Etude et de Recherche sur les Médicaments Vétérinaires et les Désinfectants, La Haute-Marche, BP90203, F-35302 Fougères Cedex, France
,
S. Gautier Community Reference Laboratory for Antimicrobial Residues, Agence Française de Sécurité Sanitaire des Aliments, Laboratoire d’Etude et de Recherche sur les Médicaments Vétérinaires et les Désinfectants, La Haute-Marche, BP90203, F-35302 Fougères Cedex, France
,
M.P. Fourmond Community Reference Laboratory for Antimicrobial Residues, Agence Française de Sécurité Sanitaire des Aliments, Laboratoire d’Etude et de Recherche sur les Médicaments Vétérinaires et les Désinfectants, La Haute-Marche, BP90203, F-35302 Fougères Cedex, France
,
V. Gaudin Community Reference Laboratory for Antimicrobial Residues, Agence Française de Sécurité Sanitaire des Aliments, Laboratoire d’Etude et de Recherche sur les Médicaments Vétérinaires et les Désinfectants, La Haute-Marche, BP90203, F-35302 Fougères Cedex, France
,
D. Hurtaud-Pessel Community Reference Laboratory for Antimicrobial Residues, Agence Française de Sécurité Sanitaire des Aliments, Laboratoire d’Etude et de Recherche sur les Médicaments Vétérinaires et les Désinfectants, La Haute-Marche, BP90203, F-35302 Fougères Cedex, France
,
E. Verdon Community Reference Laboratory for Antimicrobial Residues, Agence Française de Sécurité Sanitaire des Aliments, Laboratoire d’Etude et de Recherche sur les Médicaments Vétérinaires et les Désinfectants, La Haute-Marche, BP90203, F-35302 Fougères Cedex, France
&
P. Sanders Community Reference Laboratory for Antimicrobial Residues, Agence Française de Sécurité Sanitaire des Aliments, Laboratoire d’Etude et de Recherche sur les Médicaments Vétérinaires et les Désinfectants, La Haute-Marche, BP90203, F-35302 Fougères Cedex, France
 show all
Pages 1459-1471 | Received 07 Apr 2009, Accepted 20 Jun 2009, Published online: 18 Sep 2009

References

  • European Commission . 1990 . Council Regulation (EEC) No. 2377/90 of 26 June 1990: laying down a Community procedure for the establishment of maximum residue limits of veterinary medicinal products in foodstuffs of animal origin . Off J Eur Comm , L224 : 1 – 8 .
  • European Commission . 2002 . Commission Decision 2002/657/EC of 12 August 2002: implementing Council Directive 96/23/EC concerning the performance of analytical methods and the interpretation of results . Off J Eur Comm , L221 : 8 – 36 .
  • Gaudin , V and Sanders , P . 2007 . Guide pour la validation des méthodes biologiques de dépistage version 1 . AFSSA-LERMVD. Unpublished internal document
  • Gergov , M , Ojanperä , I and Vuori , E . 2003 . Simultaneous screening for 238 drugs in blood by liquid chromatography-ionspray tandem mass spectrometry with multiple reaction monitoring . J Chromatograph B , 795 : 41 – 53 .
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  • Hammel , YA , Mohamed , R , Gremaud , E , Lebreton , MH and Guy , PA . 2008 . Multi-screening approach to monitor and quantify 42 antibiotics residues in honey by liquid chromatography-tandem mass spectrometry . J Chromatograph A , 1177 : 58 – 76 .
  • Kaufmann , A , Butcher , P , Maden , K and Widmer , M . 2007 . Ultra-performance liquid chromatography coupled to time of flight mass spectrometry (UPLC-TOF): A novel tool for multiresidue screening of veterinary drugs in urine . Analytica Chimica Acta , 586 : 13 – 21 .
  • Muñoz , P , Blanca , J , Ramos , M , Bartolomé , M , Garcia , E , MÕndez , N , Gomez , J and Martin de Pozuelo , M . 2005 . A versatile liquid chromatography-tandem mass spectrometry system for the analysis of different groups of veterinary drugs . Analytica Chimica Acta , 529 : 137 – 144 .
  • Nielen , MWF , Van Engelen , MC , Zuiderent , R and Ramaker , R . 2007 . Screening and confirmation criteria for hormone residue analysis using liquid chromatography accurate mass time-of-flight, Fourier transform ion cyclotron resonance and orbitrap mass spectrometry techniques . Analytica Chimica Acta , 586 : 122 – 129 .
  • Stolker , AAM , Rutgers , P , Oosterink , E , Lasaroms , JJP , Peters , RJB , Van Rhijn , JA and Nielen , MWF . 2008 . Comprehensive screening and quantification of veterinary drugs in milk using UPLC-ToF-MS . Analyt Bioanalyt Chem , 391 : 2309 – 2322 .
  • Stolker , AAM , Zuidema , T and Nielen , MWF . 2007 . Residue analysis of veterinary drugs and growth-promoting agents . Trend Analyt Chem , 26 : 967 – 979 .
  • Turnipseed , SB , Andersen , WC , Karbiwnyk , CM , Madson , MR and Miller , KE . 2008 . Multi-class, multi-residue liquid chromatography/tandem mass spectrometry screening and confirmation method for drug residues in milk . Rapid Comm Mass Spectrom , 22 : 1467 – 1480 .

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