References and notes
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- Crystal data of IIId: C20H13FN2O, M r = 316.32, monoclinic, P2(1)/c, a = 8.9390(18) Å, b = 11.277(2) Å, c = 15.232(3) Å, α = 90°, β = 94.09(3)°, γ = 90(1)°, V = 1531.6(5) Å3, Z = 4, T = 293(2) K, ρ calcd = 1.372 g cm−3, μ Cu = 0.094 mm−1, F(000) = 656, total number of observed [F 2>2σ(I)] = 12 226 and independent reflections 2702 (R int = 0.0388). Numbers of restraints/parameters = 0/217, GooF = 1.085, R1 = 0.0616 and wR2 = 0.1612
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