Aerosol Flow Reactor with Controlled Temperature Gradient for In Situ Gas-Phase X-Ray Experiments—Measurements of Evaporation-Induced Self-Assembly (EISA) in Aerosols

REFERENCES

• Alonso , B. , Véron , E. , Durand , D. , Massiot , D. and Clinard , C. 2007 . New Insights into the Formation of Textures through Spray-Drying and Self-Assembly . Microporous Mesoporous Mater. , 106 : 76 – 94 .
   Web of Science ®Google Scholar
• Amenitsch , H. , Rappolt , M. , Kriechbaum , M. , Mio , H. , Laggner , P. and Bernstorff , S. 1998 . First Performance Assessment of the Small-Angle X-Ray Scattering Beamline at ELETTRA . J. Synchrotron Radiat. , 5 : 506 – 508 .
   PubMed Web of Science ®Google Scholar
• Areva , S. , Boissiere , C. , Grosso , D. , Asakawa , T. , Sanchez , C. and Linden , M. 2004 . One-Pot Aerosol Synthesis of Ordered Hierarchical Mesoporous Core-Shell Silica Nanoparticles . Chem. Comm. , 10 : 1630 – 1631 .
   Google Scholar
• Boissiere , C. , Grosso , D. , Amenitsch , H. , Gibaud , A. , Coupé , A. , Baccile , N. and Sanchez , C. 2003 . First In-Situ SAXS Studies of the Mesostructuration of Spherical Silica and Titania Particles during Spray-Drying Process . Chem. Comm. , 9 : 2798 – 2799 .
   Google Scholar
• Boissiere , C. , Grosso , D. , Chaumonnot , A. , Nicole , L. and Sanchez , C. 2011 . Aerosol Route to Functional Nanostructured Inorganic and Hybrid Porous Materials . Adv. Mater. , 23 : 599 – 623 .
   PubMedGoogle Scholar
• Bore , M. T. , Rathod , S. B. , Ward , T. L. and Datye , A. K. 2003 . Hexagonal Mesostructure in Powders Produced by Evaporation-Induced Self-Assembly of Aerosols from Aqueous Tetraethoxysilane Solutions . Langmuir , 19 : 256 – 264 .
   Web of Science ®Google Scholar
• Brinker , C. J. , Lu , Y. , Sellinger , A. and Fan , H. 1999 . Evaporation-Induced Self-Assembly: Nanostructures Made Easy . Adv. Mater. , 11 : 579 – 585 .
   Web of Science ®Google Scholar
• Bruinsma , P. J. , Kim , A. Y. , Liu , J. and Baskaran , S. 1997 . Mesoporous Silica Synthesized by Solvent Evaporation: Spun Fibers and Spray-Dried Hollow Spheres . Chem. Mater. , 9 : 2507 – 2512 .
   Web of Science ®Google Scholar
• Cagnol , F. , Grosso , D. , Soler-Illia , G. J. D. A. , Crepaldi , E. L. , Babonneau , F. , Amenitsch , H. and Sanchez , C. 2003 . Humidity-Controlled Mesostructuration in CTAB-Templated Silica Thin Film Processing. The Existence of a Modulable Steady State . J. Mater. Chem. , 13 : 61 – 66 .
   Web of Science ®Google Scholar
• Campanelli , A. R. and Scaramuzza , L. 1986 . Hexadecyltrimethylammonium Bromide . Acta Cryst. C , 42 : 1380 – 1383 .
   Google Scholar
• Doshi , D. A. , Gibaud , A. , Liu , N. , Sturmayr , D. , Malanoski , A. P. , Dunphy , D. R. , Chen , H. , Narayanan , S. , MacPhee , A. , Wang , J. , Reed , S. T. , Hurd , A. J. , Van Swol , F. and Brinker , C. J. 2003 . In-Situ X-Ray Scattering Study of Continuous Silica—Surfactant Self-Assembly during Steady-State Dip Coating . J. Phys. Chem. B , 107 : 7683 – 7688 .
   Web of Science ®Google Scholar
• Dourdain , S. , Rezaire , A. , Mehdi , A. , Ocko , B. M. and Gibaud , A. 2005 . Real Time GISAXS Study of Micelle Hydration in CTAB Templated Silica Thin Films . Physica B: Condensed Matter , 357 : 180 – 184 .
   Google Scholar
• Fan , J. , Boettcher , S. W. , Tsung , C.-K. , Shi , Q. , Schierhorn , M. and Stucky , G. D. 2008 . Field-Directed and Confined Molecular Assembly of Mesostructured Materials: Basic Principles and New Opportunities . Chem. Mater , 20 : 909 – 921 .
   Web of Science ®Google Scholar
• Fontell , K. , Khan , A. , Lindström , B. , Maciejewska , D. and Puang-Ngern , S. 1991 . Phase Equilibria and Structures in Ternary Systems of a Cationic Surfactant (C16TABr or (C16TA)2SO4), Alcohol, and Water . Colloid Polym Sci. , 269 : 727 – 742 .
   Web of Science ®Google Scholar
• Gibaud , A. , Grosso , D. , Smarsly , B. , Baptiste , A. , Bardeau , J. F. , Babonneau , F. , Doshi , D. A. , Chen , Z. , Brinker , J. C. and Sanchez , C. 2003 . Evaporation-Controlled Self-Assembly of Silica Surfactant Mesophases . J. Phys. Chem. B , 107 : 6114 – 6118 .
   Web of Science ®Google Scholar
• Grosso , D. , Cagnol , F. , Soler-Illia , G. J. D. A. , Crepaldi , E. L. , Amenitsch , H. , Brunet-Bruneau , A. , Bourgeois , A. and Sanchez , C. 2004 . Fundamentals of Mesostructuring through Evaporation-Induced Self-Assembly . Adv. Func. Mater. , 14 : 309 – 322 .
   Web of Science ®Google Scholar
• Hammersley , A. P. 1998 . FIT2D V9.129 Reference Manual, V3.1, ESRF Internal Report ESRF98HA01T ESRF, Grenoble. Available online at: http://www.esrf.eu/computing/scientific/FIT2D
   Google Scholar
• Hampsey , E. J. , Arsenault , S. , Hu , Q. and Lu , Y. 2005 . One-Step Synthesis of Mesoporous Metal-SiO2 Particles by an Aerosol-Assisted Self-Assembly Process . Chem. Mater. , 17 : 2475 – 2480 .
   Google Scholar
• Jayanthi , G. V. , Zhang , S. C. and Messing , G. L. 1993 . Modeling of Solid Particle Formation during Solution Aerosol Thermolysis: The Evaporation Stage . Aerosol Sci. Technol. , 19 : 478 – 490 .
   Web of Science ®Google Scholar
• Kammler , H. K. , Beaucage , G. , Kohls , D. J. , Agashe , N. and Ilavsky , J. 2005 . Monitoring Simultaneously the Growth of Nanoparticles and Aggregates by In Situ Ultra-Small-Angle X-Ray Scattering . J. Appl. Phys. , 97 : 054309
   Web of Science ®Google Scholar
• Kim , H.-S. , Lee , K.-H. and Kim , S.-G. 2006 . Growth of Monodisperse Silver Nanoparticles in Polymer Matrix by Spray Pyrolysis . Aerosol Sci. Technol. , 40 : 536 – 544 .
   Web of Science ®Google Scholar
• Lu , Y. , Fan , H. , Stump , A. , Ward , T. L. , Rieker , T. and Brinker , C. J. 1999 . Aerosol-Assisted Self-Assembly of Mesostructured Spherical Nanoparticles . Nature , 398 : 223 – 226 .
   Web of Science ®Google Scholar
• Marmiroli , B. , Grenci , G. , Cacho-Nerin , F. , Sartori , B. , Laggner , P. , Businaro , L. and Amenitsch , H. 2010 . Experimental Set-Up for Time Resolved Small Angle X-Ray Scattering Studies of Nanoparticles Formation Using a Free-Jet Micromixer . Nucl. Instrum. Methods Phys. Res. B , 268 : 329 – 333 .
   Google Scholar
• Mitchell , J. B. A. , di Stasio , S. , LeGarrec , J. L. and Florescu-Mitchell , A. I. 2010 . Synchrotron Radiation Studies of Additives in Combustion. I: Water . Nucl. Instrum. Methods Phys. Res. B , 268 : 1486 – 1491 .
   Google Scholar
• Moon , Y. K. , Lee , J. , Lee , J. K. , Kim , T. K. and Kim , S. H. 2009 . Synthesis of Length-Controlled Aerosol Carbon Nanotubes and Their Dispersion Stability in Aqueous Solution . Langmuir , 25 : 1739 – 1743 .
   PubMed Web of Science ®Google Scholar
• Rao , R. G. V. , Lopez , G. P. , Bravo , J. , Pham , H. , Datye , A. K. , Xu , H. F. and Ward , T. L. 2002 . Monodisperse Mesoporous Silica Microspheres Formed by Evaporation-Induced Self-Assembly of Surfactant Templates in Aerosols . Adv. Mater. , 14 : 1301 – 1304 .
   Google Scholar
• Ravichandran , R. 2009 . Nanotechnology-Based Drug Delivery Systems . Nanobiotechnol , 5 : 17 – 33 .
   Google Scholar
• Sanchez , C. , Rozes , L. , Ribot , F. , Laberty-Robert , C. , Grosso , D. , Sassoye , C. , Boissiere , C. and Nicole , L. 2010 . “Chimie Douce”: A Land of Opportunities for the Designed Construction of Functional Inorganic and Hybrid Organic–Inorganic Nanomaterials . C. R. Chimie , 13 : 3 – 39 .
   Web of Science ®Google Scholar
• Schaefer , D. W. , Olivier , B. J. , Hurd , A. J. , Beaucage , G. B. , Ivie , J. J. and Herd , C. R. 1991 . Structure of Combustion Aerosols . J. Aerosol Sci. , 22 : 447 – 450 .
   Web of Science ®Google Scholar
• Sen , D. , Spalla , O. , Taché , O. , Haltebourg , P. and Thill , A. 2007 . Slow Drying of a Spray of Nanoparticles Dispersion: In Situ SAXS Investigation . Langmuir , 23 : 4296 – 4302 .
   PubMed Web of Science ®Google Scholar
• Shyjumon , I. , Rappolt , M. , Sartori , B. , Amenitsch , H. and Laggner , P. 2008 . Novel In Situ Setup to Study the Formation of Nanoparticles in the Gas Phase by Small Angle X-Ray Scattering . Rev. Sci. Instrum. , 79 : 043905
   Web of Science ®Google Scholar
• Shyjumon , I. , Rappolt , M. , Sartori , B. , Cacho-Nerin , F. , Grenci , G. , Amenitsch , H. and Laggner , P. Mesostructured Si-Particles Studied by Comparison of Gas Phase and Powder Deposit X-Ray Diffraction . Submitted
   Google Scholar
• Tsapis , N. , Bennett , D. , Jackson , B. , Weitz , D. A. and Edwards , D. A. 2002 . Trojan Particles: Large Porous Carriers of Nanoparticles for Drug Delivery . Proc. Nat. Acad. Sci. U. S. A. , 99 : 12001 – 12005 .
   PubMed Web of Science ®Google Scholar
• Venkataraman , N. V. and Vasudevan , S. 2001 . Hydrocarbon Chain Conformation in an Intercalated Surfactant Monolayer and Bilayer . Proc. Indian Acad. Sci. (Chem. Sci.) , 113 : 539 – 558 .
   Google Scholar
• Wise , M. E. , Biskos , G. , Martin , S. T. , Russell , L. M. and Buseck , P. R. 2005 . Phase Transitions of Single Salt Particles Studied Using a Transmission Electron Microscope with an Environmental Cell . Aerosol Sci. Technol. , 39 : 849 – 856 .
   Web of Science ®Google Scholar
• Zana , R. 1995 . Aqueous Surfactant–Alcohol Systems: A Review . Adv. Coll. Interf. Sci. , 57 : l – 64 .
   Google Scholar